feoohcbc纳米复合材料的制备及性能研究word格式论文.docx

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feoohcbc纳米复合材料的制备及性能研究word格式论文.docx

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feoohcbc纳米复合材料的制备及性能研究word格式论文

AbstractFeOOHisanexcellentsemiconductormaterialwithstablechemicalproperties.TherearenumeroushydroxylgroupsinthesurfaceofFeOOH,whichhasawiderangeofusesincatalysis,adsorption,pigmentsandmagneticmaterials.However,FeOOHnanoparticlesareapttoagglomerateduetonanometersizeeffect.Therefore,preventingaggregationandimprovingtherecycleabilityhasaveryimportantimpactontheirphysicalandchemicalpropertiesandapplicationperformance.Inthestudy,carbonizedbacterialcellulose(CBC)isahigh-puritycarbonfiberwiththree-dimensionalnetworkprovidinganidealplatformforthedepositionofmetalandmetaloxidenanoparticles,actingasthecarrier,byinsituhydrolysisofFeCl3?6H2Otopreparethree-dimensionalnetworkofporousFeOOH/CBCnanocompositeandstudyitsproperties.Themaincontentsareasfollows:PreparationofFeOOH/CBCnanocomposite.FeOOH/CBCnanocompositewassuccessfullypreparedwithnanometer-scaleFeOOHloadedonthesurfaceofcarbonizedbacterialcellulose(CBC)byhydrolysisofFeCl3?6H2O.ThestructureandmorphologyofFeOOH/CBCnanocompositewerecharacterizedusingX-raydiffraction(XRD),fouriertransforminfraredspectrometer(FI-IR),brunauer-emmett-teller(BET),fieldemissionscanningelectronmicroscopy(FE-SEM),transmissionelectronmicroscopy(TEM)andhighresolutiontransmissionelectronmicroscopy(HRTEM).TheresultsshowthatFeOOH/CBChasauniquethree-dimensional(3D)porousnetworkstructure.FeOOHnanoparticleswithanaveragelengthof120nm,wideof30nmareshuttle-like.AdsorptionpropertiesofFeOOH/CBCnanocompositeformethylorange.TheadsorptionpropertiesofFeOOH/CBCnanocompositeformethylorange(MO)werecharacterizedbyusingUV-Vis.Aseriesofbatchexperimentswereperformedtoinvestigatethein?uenceofadsorbentdosage,contacttime,adsorptionkinetics,adsorptionthermodynamics,pHvaluesandrecycletimesonMOremovalunderthesameconditions.Theresultsshowedthattheadsorptionequilibriumofas-preparedFeOOH/CBCnanocompositeformethylMOwasachievedwithinonehour,withthemaximumadsorptioncapacityforMOreaching107.68mg/gatpH6.0and30℃.As-preparedFeOOH/CBCnanocompositemaintainshighadsorptionactivitiesafterfourtim