酒精蒸馏节能提质技术改造——两塔进料四塔差压蒸馏工艺的应用-transformation of energy-saving and quality-improving technology for alcohol distillation - application of differential pressure distillation process with two towers feeding and four towers.docxVIP

学位论文独创性声明本人声明，所呈交的学位论文系在导师指导下本人独立完成的研究成果。文 中引用他人的成果，均已做出明确标注或得到许可。论文内容未包含法律意义上 已属于他人的任何形式的研究成果，也不包含本人已用于其他学位申请的论文或 成果，与我一同工作的同志对本研究所做的任何贡献均已在论文中作了明确的说 明并表示谢意。论文作者签名：日期：年月日学位论文知识产权权属声明本人在导师指导下所完成的论文及相关的职务作品，知识产权归属齐鲁工业 大学。齐鲁工业大学享有以任何方式发表、复制、公开阅览、借阅以及申请专利 等权利，同意学校保留并向国家有关部门或机构送交论文的复印件和电子版，本 人离校后发表或使用学位论文或与该论文直接相关的学术论文或成果时，署名单 位仍然为齐鲁工业大学。论文作者签名：日期：年月日导 师 签 名：日期：年月日3摘要酒精行业生产普级食用酒精蒸馏工段一般是双塔流程，但双塔流程一般蒸汽 消耗量较高，且质量也不是很稳定，随着酒精质量新标准的颁布，双塔蒸馏质量 已经难以达标。本文主要论述了本企业年产 6 万吨普级食用酒精采用两塔蒸馏改 造为一种新型节能的两塔进料四塔差压蒸馏工艺，即采用两个粗塔、两个精塔， 通过两塔进料四塔差压，实现了各塔塔顶酒精蒸汽热能利用，减少了加热蒸汽用 量，节省蒸汽显著，由蒸馏吨酒精耗蒸汽 2.9 吨降至 1.23 吨，节省蒸汽 58%。 同时，采用负压操作、脱气排醛等技术措施，使普级酒精质量得以大幅提高，氧 化时间延长 5 倍、杂醇油下降了 80% 。本文还论述了一种在两塔进料四塔差压蒸馏基础上改进的优级食用酒精蒸 馏技术。该技术可同时取普级酒精和优级酒精，根据需求可以灵活生产。关键词：酒精两塔进料差压蒸馏节能降耗4AbstructThe alcohol industry produce ordinary edible alcohol ，distillation section is generally the Twin Towers process, but Twin Towers general process of steam consumption is high, and the quality is not very stable, with the new standard of alcohol quality promulgated, Twin Towers distillation quality has been difficult to reach the standard. This paper mainly discusses the general level of enterprises with an annual output of 60000 tons edible alcohol using two tower distillation for the transformation of a new energy-saving two feed the tower four tower differential pressure distillation process, using two crude tower, two fine tower by tower, two feed four tower differential pressure, realize the tower top alcohol steam heat energy utilization, reducing the amount of heating steam, The steam is saved significantly by distillation, tons of alcohol consumption of steam 2.9 tons fell to 1.23 tons, saving steam 58%. At the same time, using negative pressure operation, degassing row of formaldehyde and other technical measures, so that ordinary alcohol quality can be greatly improved, the oxidation time is prolonged by 5 times, the fusel oil dropped 80%. This paper also discusses a in the two column feed improved four tower differential pressure d