扩散连接条件对sicsic接头微观组织和力学性能的影响-influence of diffusion bonding conditions on microstructure and mechanical properties of sicsic joints.docxVIP

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扩散连接条件对sicsic接头微观组织和力学性能的影响-influence of diffusion bonding conditions on microstructure and mechanical properties of sicsic joints.docx

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扩散连接条件对sicsic接头微观组织和力学性能的影响-influence of diffusion bonding conditions on microstructure and mechanical properties of sicsic joints

AbstractThediffusionbondingprocesswasusedtoconnectSiliconcarbon(SiC)ceramics.Theeffectsofcomposition(Ti,Ni,Ti/Ni/Ti,Ti-dipping,Ti-preforming)andjoiningparameters(temperature,pressure,holdingtime)onmicrostructuresandmechanicalpropertiesofSiC/SiCjointswasstudiedbyusingX-rayDiffraction(XRD),ScanningElectronMicroscope(SEM),EnergyDispersiveSpectrometer(EDS)technologyandshearstrengthtest.TheresultsshowthatthemicrostructuresandmechanicalpropertiesofSiC/SiCjointsusingTifoil,Ti/Ni/Tifoilastheintermediatelayerwerebetterwhenjoiningtemperature,pressure,andholdingtimewere1400℃,30MPa,1h.Specificperformance:themainphasesoftheweldjointswereTiCandTi5Si3,Ni-Si;thewidthofweldjointswere38μmand45μm,andtheC,SielementofSiliconcarbonceramicsdiffusionintheintermediatelayer;theshearstrengthofSiC/SiCjointswas68.9MPaand138.0MPa,thetissueoffracturesurfacewasdense;thehardnessofSiC/SiCjointsweldwas13.7GPaand19.0GPa,elasticmoduluswas301.4GPaand352.1GPa.Inthemeantime,usingTi/Ni/Tifoilastheintermediatelayer,thedensityofweldjoints’microstructuresandbondingstrengthwerebetterthanTifoilgroup.Thedisciplinesweresameasthejoiningparameterstransformed.TheeffectsofjoiningparametersonSiC/SiCjointsperformancewerestudied,usingTi/Ni/Tifoilastheintermediatelayerweremuchbetter.Specificperformance:theSiC/SiCjoints’structurecompactnessandmechanicalpropertiesweremuchbetterwiththeincreaseoftemperature,toachievethebestat1600℃,thewidthofweldjoints,shearstrength,thehardnessofjointsweld,theelasticmodulusofjointsweldwere13μm,207.6MPa,24.7GPa,547.3GPa;theSiC/SiCjoints’structurescompactnessandmechanicalpropertieswerealsomuchbetterwiththeincreaseofpressure,toachievethebestunderthepressureof45MPa,thewidthofweldjoints,shearstrength,thehardnessofjointsweld,theelasticmodulusofjointsweldwere13μm,189.2MPa,21.2GPa,465.8GPa;butwiththeholdingtimeprolonging,theperformanceoftheSiC/SiCjoints’structurescompactnessandmechanicalpropertiesshowedthetrend.ofdecrease.Thestudyalsofoundthattheconnectiontemperaturewasthemostimportantfactorofaffecti