类水滑石复合脱氟剂的再生及吸附性能分析-regeneration and adsorption performance analysis of hydrotalcite-like compound defluorination agent.docxVIP

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类水滑石复合脱氟剂的再生及吸附性能分析-regeneration and adsorption performance analysis of hydrotalcite-like compound defluorination agent.docx

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类水滑石复合脱氟剂的再生及吸附性能分析-regeneration and adsorption performance analysis of hydrotalcite-like compound defluorination agent

AbstractAccording to the intake of fluoride，fluorine can be beneficial or harmful to the health of the human. The World Health Organization states that the concentration of fluorine ionsin drinking water shall not exceed 1.5mg/L，while China provides the concentration of F-in drinking water shall not exceed 1.0mg/L. Worldwide, especially in semi-arid areas, the hazards of fluoride in groundwater to human is a concern.This article expanded the research which have been done by our research group about hydrotalcite-like compound defluorination agent. The influence of various regeneration means: calcination, soaking in alkali liquor or acid liquor, being calcined after soaking in alkali liquor or in acid liquor or in CaCl2 solution, the results showed that the means without calcination had no significant regeneration effect, the defluorination rate of the agent that had been calcined was high, especially the agent that soaked in alkali liquor, the defluorination rate reached up to 90%. Calcined temperature 300,350,400,450,500,550,600 °C were studied, the results showed that 400 °C was the most suitable calcination temperature; calcined the saturated adsorbent in 400 °C respectively for 0.5 , 1,1.5,2,2.5,3,3.5,4 h the results showed that 2h is preferably calcined time; soaked in the NaOH solution (respectively pH = 8,9,10,11,12,13,14) 1.5h, after being washed, calcined under conditions of 400 ° C for 2h, the results showed that pH = 9 was the best condition.Fixed-bed reactor filled with the composite adsorbent was prepared to study the dynamic adsorption performance and then analysed the breakthrough curves (effluent concentration of F-1.0mg / L for breakout point), and the breakthrough curves were simulated respectively by Thomas model, shortcut model and Boltzmann model. Fixed bed reactor’s diameter was 4cm, length 20cm. The general parameters set as that the quality of the bed was 4g, flow velocity was 12mL/min, the initial concentration of F- was 10 mg / L ,the t