利用电石渣和盐湖氯化镁制备氢氧化镁的分析-analysis of magnesium hydroxide preparation by carbide slag and salt lake magnesium chloride.docxVIP

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利用电石渣和盐湖氯化镁制备氢氧化镁的分析-analysis of magnesium hydroxide preparation by carbide slag and salt lake magnesium chloride.docx

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利用电石渣和盐湖氯化镁制备氢氧化镁的分析-analysis of magnesium hydroxide preparation by carbide slag and salt lake magnesium chloride

AbstractHigh purity magnesium hydroxide was prepared by using carbide slag and salt magnesium chloride as raw materials. The extraneous component of carbide slag was complex, thus use carbide slag reacted with sodium sulfate and ammonium chloride respectively, and magnesium hydroxide was obtained through the reaction of magnesium chloride and the alkali that was obtained through the above reaction. Two kinds of technologies of preparing magnesium hydroxide were got through single factor experiment and orthogonal experiment. The purity of magnesium hydroxide was measured by using ICP and the EDTA titration method, and characters of product were carried out using XRD, SEM.The optimally technological conditions of using sodium sulfate were listed bellow. Saturated sodium sulfate solution put 20 hours with carbide slag quietly, and the reaction temperature of the filtrate and magnesium chloride solution was 40℃ and the reaction time 35 minutes. The purity of product was above99.07 percent, the result of XRD completely consistent with standard atlas of magnesium hydroxide, and the result of SEM showed that the product was flaky and the grain size was about1μm.The optimally technological conditions of using ammonium chloride were listed bellow. The mol rate of ammonium chloride and magnesium chloride was 5.0, the concentration of magnesium chloride 2.0mol/L，the reaction time 60 minutes, the reaction temperature at 25℃, the ageing time 2 hours. In these conditions, the productive rate of magnesium hydroxide was above 89.08 percent, the purity of product above 99.09 percent, the result of XRD completely consistent with standard atlas of magnesium hydroxide, magnesium hydroxide agreed with the HG/T3607-2007 standard,and the result of SEM showed that the product was flaky and the grain size was about 1 μm.Compared with the two methods, dissolvability of calcium hydroxide in sodium sulfate and carbide slag was small, effecting the productive rate of magnesium hydroxide, big wa