高温介孔脱硫剂的制备和高硫容性质的分析-preparation of high temperature mesoporous desulfurizer and analysis of its high sulfur content properties.docxVIP
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高温介孔脱硫剂的制备和高硫容性质的分析-preparation of high temperature mesoporous desulfurizer and analysis of its high sulfur content properties
目录第一章文献综述........................................................................................................................11.1研究背景.........................................................................................................................11.2传统煤气脱硫技术.......................................................................................................61.2.6单乙醇胺法(索尔菲班法)..............................................................................81.3热煤气脱硫技术............................................................................................................81.3.1锰基脱硫剂........................................................................................................91.3.2铁基脱硫剂......................................................................................................111.4载体MCM-41131.5论文的提出与内容....................................................................................................18第二章实验部分.......................................................................................................202.1药品与仪器...................................................................................................202.1.1实验药品...........................................................................................202.1.2实验仪器...........................................................................................212.2载体和脱硫剂的制备..................................................................................222.2.1水玻璃模数比的测定.......................................................................222.2.2MCM-41的合成222.2.3Fe掺杂的Mn基脱硫剂的制备232.2.4铝溶胶的制备...................................................................................232.2.5放大成型脱硫剂的制备...................................................................232.3脱硫剂表征..................................................................................................242.3.1低温氮气吸附表征(BET)242.3.2X射线衍射(XRD)262.3.3X射线光电子能谱(XPS)272.3.4高分辨率透射电镜(HRTEM)272.3.5激光拉曼光谱(LRS)272.4脱硫剂脱硫性能的测试.............
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