tipb02耐酸阳极电催化性及稳定性分析-electrocatalysis and stability analysis of tipb 02 acid-resistant anode.docx

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tipb02耐酸阳极电催化性及稳定性分析-electrocatalysis and stability analysis of tipb 02 acid-resistant anode.docx

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tipb02耐酸阳极电催化性及稳定性分析-electrocatalysis and stability analysis of tipb 02 acid-resistant anode

太原理T太学硕士研究生学校论文STUDYONELECTROCATALYTICPERFORMANCEANDSTABILITOFTilPb02PROOF-ACIDANODEABSTRACTTi-basedoxideelectrodesinelectrochemicalindustry，suchasthedegradationofpollutantandelectrochemicalsynthesis，areveηpromlsmg.However，whiletitaniumanodeswereusedinthec臼eofstrongacidelectrolyte，thetitaniumdioxideinsulatorwasformedbecauseofactiveoxygenofanode，theconductivi句randbindingofanodewereweakened.Additionofoxidessolidsolutionintermediateprovidesanewmethodtoimprovecorrosionresistance.Theelectrocatalyticofelectrodescanwerediscussedquantificationallybyfractaldimensionandkineticparameters.Thereforeitisimportanttos阳dyelectrocatalyticperforrnanceandstabilityofproofacidanode.Ti/Sn02+Sb20JPb02anodew部preparedbymeansofthethermaldecompositionandelectrodepositiontechnology.Thesurtà.cemorphologyandmicrostructureofthecoatingwerecharacterizedbymeansofSEM.ThecyclicvoltammetryandkineticsparametersweremeasuredbythreeelectrodessystemIlIinacidsolutionunderdi仔怪rentscanningspeed.The仕actalgeometrγtheorywasintroducedintotitaniumbasedoxideelectrodesystem，thecorrelationbetween太原理J:大学硕士研究生学位论文surf与cefractaldimensionoftheoxideelectrodeandtheelectrocatalyticperformancehasbeendiscussed.The仕actaldimensionsofelectrodesurfacewerequantificationallycalculatedunderthedi的rentSbdopingconcentrationsimultaneouslybasedonthecorrelationbetweendifferentscanrateandpe成current，therelationbetween仕actaldimensionandelectrocatalyticperformanceofevolutionoxygeninacidsolutionwasdiscussedemphatically.ConductivityofelectrodewasinvestigatedbyACimpedanceexperiment.Theanticipatedservicelifeoftheoxideanodeswereinspectedbyacceleratedlifemethodin1.0mol/LH2S04solutionat4Acm气Theconc1usionsareasfollows:ThesurfaceoftheSn02+Sb204electrodehavethecηstalstructure，canformagoodsolidsolutionwhichcaneffectivelypreventoxygenatedspeciestransporttowardthetitaniumsubstrate.TheactivatedlayeroftheTi/Sn02+Sb20JPb02anodewithahighsurfaceareaandashapeofmushroomhaveagoodelectrocatalyticperformance.Theobtainedresultsfromthecyclicvoltammetrymeasurementsshowe