SnO 2纳米粉体的制备及其气敏性能研究.kdh.pdfVIP

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SnO 2纳米粉体的制备及其气敏性能研究.kdh.pdf

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26 2 Vol.26 No.2 2007 2 ELECTRONIC COMPONENTS AND MATERIALS Feb. 2007 SnO 2 1 2 Sn sol-gel SnO2 XRDTEM 25 nm 300 SnO2 5×10–5 805 3 s 7 s SnO2 sol-gel 0645.542 A 100102-0031-03 Preparation of SnO nanopowder by sol-gel method and its 2 gas sensitivity properties 1 2 NIU Xin-shu , DU Hui (1.College of Chemistry Environmental Science, Henan Normal University, Henan Key Laboratory of Environmental Pollution Control, Xinxiang 453007, China; 2. Department of Chemical Engineering, Anyang Institute of Technology, Anyang 455000, China) Abstract: SnO powders were synthesized by sol-gel method in the system of citric acid with Sn grain as the starting 2 materials. The structure and crystal state of the powders were determined by XRD method. The shape and size were analyzed by means of JEM100SX TEM. The results show this tetragonal system oxide is spherical with the mean grain size of 25 nm and its dispersity is good. The study of sensor’s gas sensing characteristic shows SnO2 has higher sensitivity 805to 50×10–6 Cl2 at 300 when the precursor has been treated at 550 . At the same time, its selectivity is also good. The response time and recovery time are 3 s and 7 s, respectively. Key words: electron technology; SnO nanopowder; sol-gel method; gas-sensoring material; Cl 2 2 SnO2 1968