镁合金微弧氧化深色膜的制备及性能分析-preparation and performance analysis of magnesium alloy micro-arc oxidation dark film.docxVIP
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镁合金微弧氧化深色膜的制备及性能分析-preparation and performance analysis of magnesium alloy micro-arc oxidation dark film
沈阳理工大学硕士学位论文filmwasmainlycomposedofMgO,MgAl2O4andCu3MgO4;theblackishgreenceramicfilmwasmainlycomposedofMgO,SiO2,Mg2SiO4,CuN6andCuSiO3·H2O.Themainreasonofcolor-displayisthatVoxideorCuoxideexistsinthefilm.Corrosionexperimentandelectrochemicaltreatmentshowedthattheanticorrosionpropertyofthefuscousceramicfilmswasimproved.Inthispaper,anewmethod,chemicalconversionandmicro-arcoxidation,waspresentedtopreparethefuscousceramicfilms.Thegrayblackoxidationfilmanddarkredoxidationfilmwereobtainedthroughthemethod.Theeffectsofprocessofchemicalconversionandmicro-arcoxidationonthecolorofthefilmswereinvestigated.Thetechnologyconditionsofthefuscousceramicfilmswereoptimizedthroughorthogonaltest.ThechemicalconversiontechnologyconditionsforpreparingthegrayblackoxidationfilmisNaMoO4230g/L,pH=3,T=60℃,t=8min;ThechemicalconversiontechnologyconditionsforpreparingdarkredoxidationfilmisKMnO450g/L,NH4H2PO4100g/L,T=50℃,t=11min.Themicro-arcoxidationtechnologyconditionsbothareNa2SiO310g/L,NaOH5g/L,t=10~20min.TheSEMresultsshowedtheuniformandcompactfilmswereobtained.TheXRDresultsshowedgrayblackoxidationfilmwasmainlycomposedofSiO2,Mo9O26,MgSiO3andMg2SiO4;darkredoxidationfilmwasmainlycomposedofSiO2、MnO、MnP、MgSiO3andMg2SiO4.Electrochemicaltreatmentshowedthatthecorrosionresistingpropertyofthebrunetceramicfilmswasverygood.Thismethodhasnotseenintheliterature.Inprocessofmicro-arcoxidation,theinfluenceofultrasonicwaveonMAOfilmswasinvestigated.Theresultsshowedthepropertiesofthefilmswereimproved.Keywords:micro-arcoxidation;magnesiumalloys;fuscousceramicfilm;chemicalconversion;corrosionresistingproperty沈阳理工大学硕士学位论文原创性声明本人郑重声明:本论文的所有工作,是在导师的指导下,由作者本人独立完成的。有关观点、方法、数据和文献的引用已在文中指出,并与参考文献相对应。除文中已注明引用的内容外,本论文不包含任何其他个人或集体已经公开发表的作品成果。对本文的研究做出重要贡献的个人和集体,均已在文中以明确方式标明。本人完全意识到本声明的法律结果由本人承担。作者(签字):日期:年月日学位论文版权使用授权书本学位论文作者完全了解沈阳理工大学有关保留、使用学位论文的规定,即:沈阳理工大学有权保留并向国家有关部门或机构送交学位论文的复印件和磁盘,允许论文被查阅和借阅。本人授权沈阳理工大学可以将学位论文的全部或部分内容编入有关数据库进行检索,可以采用影印、缩印或其它复制手段保存、汇编学位论文。(保密的学位论文在解密后适用本授权书)学位论文作者签名:指导教师签名:日期:日期:第1章绪论1.1镁及镁合金的性质与应用1.1.1镁及镁合金概述
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