毕业设计论文 (乙醇乙醚的多组分精馏多线进料的精馏塔设计）.docVIP

年产1500t乙酸乙酯车间工艺设计 PAGE III PAGE PAGE II PAGE I 摘 要 乙酸乙酯是一种重要的有机化工产品，目前国内主要的生产方法是以98%浓硫酸为催化剂连续生产的乙酸、乙醇直接酯化工艺路线。本设计对乙酸乙酯直接酯化工艺进行了分析设计，采用反应精馏塔提高原料转化率，利用原料产物进行恒沸精馏来提高产品的浓度。通过物料、能量恒算和设备计算得到工艺参数，本文对多组分精馏、多线进料的精馏塔进行了设计，最后得到工艺流程图和设备图。 关键词：直接酯化法，恒沸液，反应精馏，流程设计，衡算 ABSTRACT Ethyl acetate is an important organic chemical products, domestic production method is with 98 percent concentrated sulphuric acid as a catalyst to and with acetic acid, ethanol as raw materials directly esterification process line. The design get an analysis to the ethyl acetate direct esterification, use of distillation columns reaction to increase of conversion rate of raw materials, and use of azeotropic distillation of raw materials products to increase the concentration of products. The process parameters were obtained by the equilibrium calculation of materials, energy and equipment. In this paper, multi-component distillation, multi-feed the distillation tower was designed. In the end the process flow chart. KEYWORDS：Direct Rsterification, Constant boiling liquid, Reactive distillation, Process Design, Balance calculation 目 录 TOC \o 1-3 \h \z \u HYPERLINK \l _Toc200437171 第一章 概述 PAGEREF _Toc200437171 \h 1 HYPERLINK \l _Toc200437172 1.1产品国内外需求动向 PAGEREF _Toc200437172 \h 1 HYPERLINK \l _Toc200437173 1.1.1国外生产及消费市场 PAGEREF _Toc200437173 \h 1 HYPERLINK \l _Toc200437174 1.1.2我国内生产及消费市场 PAGEREF _Toc200437174 \h 2 HYPERLINK \l _Toc200437175 1.2产品生产方法简述 PAGEREF _Toc200437175 \h 2 HYPERLINK \l _Toc200437176 1.3 设计任务说明 PAGEREF _Toc200437176 \h 3 HYPERLINK \l _Toc200437177 1.4 建厂选址 PAGEREF _Toc200437177 \h 3 HYPERLINK \l _Toc200437178 第二章 工艺方法和流程的确定 PAGEREF _Toc200437178 \h 5 HYPERLINK \l _Toc200437179 2.1现有生产工艺过程及状况 PAGEREF _Toc200437179 \h 5 HYPERLINK \l _Toc200437180 2.2现有工艺方法的比较选择 PAGEREF _Toc200437180 \h 5 HYPERLINK \l _Toc200437181 2.2.1直接酯化法 PAGERE