酸奶中苯及苯同系物气相色谱-质谱检测方法的建立-食品安全质量.PDF

7 3 Vol. 7 No. 3 2016 3 Journal of Food Safety and Quality Mar. , 2016 - * 王俊平 , 郭 楠, 王 硕 (, 300457) 摘 要: 目的 -方法 , , 10 mL, NaCl 2.0 g, 5000 r/min, 20 min, 60 ℃ 结果 , () : 10.873.070.340.554.867, : 20.050.010.010.05 μg/L( S/N 3), : 50.120.050.060.15 μg/L (S/N 10)82%~104%, (RSD)4% 6 , 4~24 μg/L 结论 , , 关键词: ; ; ; - Detection of benzene and benzologue in yogurt by gas chromatography-mass spectrometry * WANG Jun-Ping , GUO Nan, WANG Shuo (Food Engineering and Biotechnology Faculty, Tianjin University of Science and Technology, Tianjin 300457, China) ABSTRACT: Objective To establish a qualitative and quantitative method for the determination of BTEX (benzene, toluene, xylene, acetophenone) in yogurt by headspace solid-phase microextraction and gas chromatography mass spectrometry technology. Methods The headspace solid-phase microextraction conditions were as follows: sample volume 10 mL, amount of NaCl 2.0 g, extraction time 20 min, and extraction temperature 60 ℃ . Relative correction factor was used for the quantitative anal