材料表征教学料 sem.ppt

Dr. Di Wu, Nanjing University * Backscattered Kikuchi Pattern Kikuchi patterns change with the change of grain orientation. Lattices with less symmetry have more complex patters. augite monoclinic, C2/c Dr. Di Wu, Nanjing University * Backscattered Kikuchi Pattern augite monoclinic, C2/c Kikuchi patterns change with the change of grain orientation. Lattices with less symmetry have more complex patters. Dr. Di Wu, Nanjing University * Backscattered Kikuchi Pattern augite monoclinic, C2/c Kikuchi patterns change with the change of grain orientation. Lattices with less symmetry have more complex patters. Dr. Di Wu, Nanjing University * Electron Backscatter Diffraction The left figure shows an EBSD camera attached on a SEM. CCD camera Dr. Di Wu, Nanjing University * Effect of Sample Tilt The larger the tilt angle, the stronger the electron signals. However, the smaller the tilt angle, the better the resolution perpendicular to the tilt axis. Dr. Di Wu, Nanjing University * EDS Qualitative Analysis EDS qualitative analysis is based on Moseley formulism of characteristic X-rays. ? is the frequency of characteristic X-rays, Z is the atomic number, K and ? are constants, and c is speed of light in vacuum. Dr. Di Wu, Nanjing University * EDS Qualitative Analysis The wavelength (energy) of characteristic X-rays varies monotonically with atomic number Z. The energy of the X-rays does not change with accelerating voltages of the incident electron beam. Dr. Di Wu, Nanjing University * Qualitative Analysis The vertical axis is the number of pulses (the number of photons detected), the horizontal axis is the pulse height (the energy of photons). The number of pulses depends on the concentration of the elements, while the pulse height is determined by the atomic number of the corresponding elements. Dr. Di Wu, Nanjing University * Quantitative Analysis Quantitative results are readily obtained without standards. The accuracy of standardless quantitative analysis is highly sa