多壁碳纳米管分散固相萃取-液质联用技术测定茶叶中草甘膦草铵膦.PDF

5 4 Vol. 5 No. 4 2014 4 Journal of Food Safety and Quality Apr. , 2014 - 1 1 1 1 1* 1 2 冯月超 , 马立利 , 贾 丽 , 张春梅 , 刘 艳 , 范筱京 , 潘灿平 (1. , , 100089; 2. , 100193) 摘 要: 目的 方法 , (MWCNTS)N-(PSA) , 9-(FMOC-Cl)BEH C18 , -4 mmol , (ESI+), (MRM), 结果 0.1∼1 μg/mL, 0.999, 10 μg/kg, , 0.250.501.00 mg/kg, 95%~116%, 98%~118%, 74%~84%, 6.79%(n=6)结论 , 关键词: ; ; ; ; ; ; Determination of glyphosate, glufosinate and aminomethylphonic acid residues in tea by liquid chromatography-tandem mass spectrometry using multi-walled carbon nanotubes as dispersive solid-phase extraction sorbent 1 1 1 1 1* 1 2 FENG Yue-Chao , MA Li-Li , JIA Li , ZHANG Chun-Mei , LIU Yan , FAN Xiao-Jing , PAN Can-Ping (1. Beijing Engineering Research Center of Food Safety Analysis, Beijing Center for Physical and Chemical Analysis, Beijing 100089, China; 2. College of Science, China Agricultural Uniwersity, Beijing 100193, China) ABSTRACT: Objective An ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) analysis method was established for simultaneous determination of glyphosate, glufosinate and aminomethyl- phonic acid (AMPA) in tea. Methods Th