气相色谱法测定食品接触材料中12种单体的迁移量-包装工程.PDF

鍖呰宸ョ▼ 绗?6鍗 绗?1鏈 36 PACKAGINGENGINEERING 2015骞?鏈 姘旂浉鑹茶氨娉曟祴瀹氶鍝佹帴瑙︽潗鏂欎腑12绉嶅崟浣撶殑杩佺Щ閲 1 1 1 1 2 1 2 鏉庤嫳 锛屾潕鎴愬彂 锛屽瓩灏忛 锛岄檲鏃緣 锛岄檲鏋濇 锛岃嫃涓 锛屽惔缁嶇簿 锛?.娣卞湷鍑哄叆澧冩楠屾鐤眬锛屾繁鍦 518067锛?.娣卞湷妫€楠屾鐤瀛︾爺绌堕櫌锛屾繁鍦 518067锛 鎽樿锛氱洰鐨勭洰鐨 寤虹珛鍚屾椂娴嬪畾椋熷搧鎺ヨЕ鏉愭枡涓?2绉嶄笝鐑吀閰拰鐢插熀涓欑儻閰搁叝绫诲崟浣撹縼绉婚噺鐨勫垎鏋愭柟 娉曘€傛柟娉曟柟娉 閲囩敤姘淬€佷箼閰革紙璐ㄩ噺鍒嗘暟涓?%锛夈€佷箼閱囷紙浣撶Н鍒嗘暟涓?0%锛夊拰姗勬娌规蹈娉￠鍝佹帴瑙︽潗鏂欙紝灏 寰楀埌鐨勬按銆佷箼閰搞€佷箼閱囩瓑姘存€фā鎷熺墿鍜屾﹦姒勬补妯℃嫙鐗╁垎鍒粡杩?0锛?0 鈩冮《绌哄姞鐑?0min鍚庯紝閫氳繃 DB-624鐭宠嫳姣涚粏绠℃煴锛?0m脳0.32mm脳1.8 渭m锛夊垎绂伙紝椤剁┖杩涙牱鍒嗘瀽锛屾阿鐏劙绂诲瓙鍖栨娴嬪櫒妫€娴嬶紝淇 鐣欐椂闂村畾鎬э紝宄伴潰绉畾閲忋€傜粨鏋滅粨鏋 12绉嶅崟浣撳湪0.1~50mg/L锛堟按鎬фā鎷熺墿锛夊強0.5~50mg/kg锛堟﹦姒勬补妯℃嫙 鐗╋級鐨勬祿搴﹁寖鍥村唴鍛堣壇濂界嚎鎬э紝鐩稿叧绯绘暟R澶т簬0.999銆傚姞鏍囧洖鏀剁巼涓?9.3%~109.6%锛岀浉瀵规爣鍑嗗亸宸 涓?.13%~7.55%銆傜粨璁虹粨璁 璇ユ柟娉曞墠澶勭悊绠€渚匡紝鍒嗙搴﹀ソ锛屽垎鏋愮伒鏁忓害楂橈紝婊¤冻椋熷搧鎺ヨЕ鏉愭枡涓?2绉嶄笝 鐑吀閰拰鐢插熀涓欑儻閰搁叝绫诲崟浣撹縼绉婚噺鐨勫垎鏋愯姹傘€ 鍏抽敭璇嶏細鏈夋瘨鏈夊鍗曚綋锛涜縼绉婚噺锛涢鍝佹帴瑙︽潗鏂欙紱椤剁┖姘旂浉鑹茶氨娉 涓浘鍒嗙被鍙凤細TS207 鏂囩尞鏍囪瘑鐮侊細A 鏂囩珷缂栧彿锛?001-3563锛?015锛?1-0036-06 Determination of Migration of 12 Monomers in Plastic Food Contact Materials by Gas Chromatography LIYing 锛孡ICheng-fa 锛孲UNXiao-ying 锛孋HENXu-hui 锛孋HENZhi-nan 锛孲UDan 锛學UShao-jing1 1 1 1 2 1 2 锛?. Shenzhen Entry-Exit Inspection and Quarantine Bureau锛孲henzhen 518067锛孋hina 锛 2. Shenzhen Academy of Inspection and Quarantine锛孲henzhen 518067锛孋hina锛 ABSTRACT 锛歍his experiment established an effective analytical method for the simultaneous determination of the migration amount of 12 ester monomers including acrylic esters and metacrylic acid esters in food contact materials by gas chromatography (GC). Using water, 3% acetic acid, 10% ethanol and olive oil soaked food contact materials, the obtained