高含量天然生育酚制备工艺研究-生物化工专业论文.docxVIP

淅江大学硕士学位论文：高音量天然生育酚制备工艺研究‘2∞7)ABSTRACT 淅江大学硕士学位论文：高音量天然生育酚制备工艺研究‘2∞7) ABSTRACT Thepreparationofnaturaltoeophe∞olsisflU恤elinvestigatedonthebasis ofthe work that has been done by也e Nati01)al I．aboratory of Secondary Resotlrees Chemical Engineeritl舀 Study tlae effect ofwater content in solvent(ethan01)on 1he a‘I哪tion capability to improve岫traditional process．Adsorption brea1【【hrough tinYeS w∽obtained, which WOIe determined 011 n adsorption column of inner diameter 2．0 cm,resin packing lleighI 25 Gill．The effects oftemperature，toeopherol concentration and flow rate oil adsoTption breakthrough cllltVe$have also been studied when ethanol and 95％ ethanol Wele used∞solvent．田le results indiented that the watereon．tent in ethanol had great influence on tho adsolption process．The optimum operation eoladitiom w讹∞follows：tealaperature 40(2．toeopherol concentration 50 mg／ml,flow rate l～1．5 BV／h when ethaaol WaS used as solvent；and temporatt口e 40(2。toeopherol coneenmation 60 mgCml．flow rato 1～1．5 BV／h when 95％ethanol was med勰solvent, respeel：ively． Study the regeneration technology of adsorption resin,the results∞follows call be obtained：the best solvent is metlumol and it is difficult to USe only one solvent in the process when methyl esterit赴ntion products used∞raw material‘,．It is potential to use single solvent when 50％tocoplaerols used∞raw material,a． The new proce89 of preparatiorl of natural tocophcrols by using the mixed solvent methanol and hexane(IO：I)h笛be∞studied．The optimum operation eonditiom WCle勰follows：methanol／hwxaae(10：1)，temperature 400，concentration 1 g／lO ral，the maximal load 15 g 50％tocophcrols matorials／94．2 ml resin．TheⅡ -toeopherol cm also be obtained by adsorption process or oxtr-aefion and the specific fotatiortofproductis30．27。，whichishiOlcrtlaantheproductmadebytransformation． Keywordls；lV．mluralToeopherols·Water cOn细tlnEthortai·RegeneratiHteelanology，| Adsorption technob舒 新江大学硬士学位论文t高音量天然生育酚制备工艺研究(2007)日!『百 新江大学硬士学位论文t高音量天然生育酚制备工艺研究(2007) 日!『百 天然生育酚(