原料蛋黄粉中锌含量的检测-食品安全质量检测学报.PDF

4 5 Vol. 4 No. 5 2013 10 Journal of Food Safety and Quality Oct. , 2013 * 其其格 , 乌尼尔, 高 娃, 满都呼, 常建军 (, 011500) 摘 要: 目的 方法 , 5 mL , 2 mL 5 min, , 1 mL, 2%50 mL , 结果 0.092 mg/kg, R 0.999 , 97.2%~101.5%结论 , 关键词: ; ; Detection of zinc content in raw egg yolk powder * QI Qi-Ge , WU Ni-Er, GAO Wa, MAN Du-Hu, CHANG Jian-Jun (Inner Mongolia Mengniu Dairy Industrial Co . Ltd ., Hohhot 011500, China) ABSTRACT: Objective To establish a simple detection method for zinc content in the egg yolk powder, and get the accurate results. Methods The method was performed by microwaving a certain amount of egg yolk powder for testing, and adding 5 mL of concentrated nitric acid with slow shaking a few times, then adding 2 mL of hydrogen peroxide for 5 min. Tightened the lid and put into the microwave digestion apparatus for digestion, and caught the acid to 1 mL after cooling in a perforated-style hot plate, then transferred to a 50 mL volumetric flask with 2% hydrochloric acid solution by shaking. Results The assay detection limit was 0.092 mg/kg, the element within the linear range correlation coefficient R was 0.999 or more, the recovery was 97.2%~101.5%. Conclusion The detection method is simple, accurate and reliable. KEY WORDS: egg yolk powder; zinc; microwave digestion , , [2-3] , , , , ,