鸡肉中多种磺胺兽药残留量测定高效液相色谱-电化学检测法.PDFVIP

21 4 Vol. 21 No. 4 2002 7 FENXI CESHI XUEBAO( Journal of Instrum ntal Analysis) Jul. 2002 - 王建华, 林黎明, 陈长法 ( , 266002) : ; , , KH2PO4 , , , C18 , - 0. 01 mol/ L KH2PO4 ( pH 6, 25 B 75) , 1. 0 V; , ( ECD) , ECD 0. 02 ng, 0. 06 ng, 0. 07 ng : ; ; ; ; : TS251. 55 : A : 1004- 4957( 2002) 04- 0079- 03 ( SAs) , , , 100 Lg/ kg[ 1] GC GC- MS , [ 2] [ 3] , , [ 4] ( FSIS) ( TLC) , , , [ 5 ] , [ 6 ] , ( ECD) ( DAD) , SA ECD DAD : 2001- 08- 05: : 2002- 03- 19 : ( 1968- ) , , , , . ( 78 ) D t rmination of Li ustilid in Radix An lica Sin nsis b SFE- Ca illar GC g g y p y 1 1 1 2 HUANG Bao_hua , ZHANG Kun , GUAN Yan_ ion , ZHOU Xiao_hui q g ( 11 Light Industry and Ch mical Engin ring School, Guangdong Univ rsity of T chnology, Guangzhou 510090, China; 21 Ex rim nt R s arch C nt r, Guan don Univ rsit of T chnolo , Guan zhou 510090, China) p g g y gy g Abstract: Ligustilid is on of th main activ constitu nts in Radix Ang lica Sin nsis. A capillary gas chro- mato ra hic m thod for th d t rmination of li ustilid was ro os d ho in to o timiz conditions for su rcritical g p g p p p g p p fluid xtraction of li ustilid . Th xtracts