基质固相分散-高压液相色谱-高分辨质谱法测定猪肉中22种磺胺类.PDF

4 1 Vol. 4 No. 1 2013 2 Journal of Food Safety and Quality Feb. , 2013 -- 22 * 徐伟东, 秦 峰 , 李晓雯, 陈桂良 ( , 201203) 摘 要: 目的 --22 , 噁 噁 方法 噁 噁 , , , 15 mL 1%: (13, v/v) , , 1 mL : 10 mmol/L (1585, v/v)1 mL , , 0.22 μm Agilent Poroshell 120 EC-C18(2.1 mm×150 mm, 2.7 μm), 结果 22 10~100 μg/kg , r0.99, /40%, 60%, 5~10 μg/kg结论 , 关键词: ; ; ; Determination of twenty-two sulfonamide residues in pork by matrix solid phase dispersion-high pressure liquid chromatography-high resolution mass spectrometry * XU Wei-Dong, QIN Feng , LI Xiao-Wen, CHEN Gui-Liang (Shanghai Institute of Food and Drug Control, Shanghai 201203, China) ABSTRACT: Objective To establish a method for determination of 22 sulfonamides in pork, including sul- fabenzamide, sulfacetamide, sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfamethazine, sulfam- erazinesulfadoxine, sulfamonomethoxine, sulfamethoxypy