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内脏和牛奶中咪唑脲苯残留量的高效液相色谱测定及液相色谱-串联
5 2 Vol. 5 No. 2
2014 2 Journal of Food Safety and Quality Feb. , 2014
-
1* 2 1 2 2 2 2
李晓娟 , 李 玮 , 陈冬东 , 艾连峰 , 郭春海 , 陈瑞春 , 王凤池
(1. , 100123; 2. , 050051)
摘 要: 目的 --
方法 1%-(1:4, v/v), Oasis WCX ,
, -结果 10 μg/kg(S/N 3), 25
μg/kg(S/N 10); LOQMRL 2MRL 6 , 72.7%~101%,
1.2%~6.9%结论 ,
关键词: ; ; ; ; -
Determination of imidocarb residue in animal tissues and milk by
HPLC and HPLC-MS/MS
1* 2 1 2 2
LI Xiao-Juan , LI Wei , CHEN Dong-Dong , AI Lian-Feng , GUO Chun-Hai ,
CHEN Rui-Chun2, WANG Feng-Chi2
(1. Chinese Academy of Inspection and Quarantine, Beijing 100123, China;
2. Hebei Entry-Exit Inspection and Quarantine Bureau, Shijiazhuang 050051, China)
ABSTRACT: Objective A method for determination of imidocarb in animal tissues and milk by
SPE-HPLC-MS/MS confirmation was developed. Methods The sample was extracted by 1% trifluoroacetic
acid-acetonitrile(1:4, v/v), purified by SPE, detected by HPLC and quantified by the external standard. Results
The LOD and LOQ of imidocarb were 10 μg/kg (S/N≥3) and 25 μg/kg (S/N≥10). The average recoveries range
of imidocarb at three levels of LOQ, MRL and 2MRL was 72.7%~101% with the relative standard deviations
(RSDs) of 1.2%~6.9%. Conlusion This method is convenient, accurat
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