反向微乳液法制备掺杂co的锰锌铁氧体及其结构性能的研究环境工程专业论文.docxVIP

矫顽力。关键词：锰锌铁氧体；Co掺杂；磁性能；微乳液；尖晶石结构 矫顽力。 关键词：锰锌铁氧体；Co掺杂；磁性能；微乳液；尖晶石结构 AbstractIn Abstract In this thesis，we use ferric chloride，manganese chloride，zinc sulfate and cobalt chloride as raw material to prepare nanomaterials doped with cobalt， manganese zinc ferrite．At the same time，make preparation of high—performance for opening a new process routes of making Mn—Zn ferrite． And for the next use of the iron vitriol dreg of yellow sodium that Jinchuan company stored．Northwest Yongxin Group for Preparation of nano-materials， high—performance coatings doped foreshadowed． In the experiment，MnZn ferrite is prepared by the reverse micro emulsion method，SO that we can control the particle size and shape．This article focuses on the impacts of the preparation with different doping content of Cop(X= 0，0．1，0．2，0．3，0．4，0．5)by micro emulsion method on the Mn Zn ferrite nanoparticles structure and its magnetic properties．And the same doping content of C02+was also studied in the condition of calcined and uncalcined to find the impacts on the Mn Zn ferrite nanoparticles structure and its magnetic properties． And characterize X—ray dj仟ractjon(XRD)，scanning electron microscopy(SEM)，vibrating sample magnetometer(VSM)and X—rayenergy dispersive spectroscopy(EDS)on CoxZno．5Mnl．xFel．504，the results show that： Successfully prepared CoxZno．5MnldFel．504 doped different content of C02+by using microemulsion method，EDS analysis shows that，element Co replaces element Zn and determined the composition and molecular formula of MnZn cobalt ferrite．With the content of element Co increasing，the content of element Mn decreases，while elements Fe and Zn basically remain the same． XRD shows that both samples calcined or uncalcined are single spinel structures without other impurity．At the same time adding moderate amount of Co”+enlarge ferrite particles in size，but excess doping make the particle size decrease．The results of the charaCterizatiOn Of XRD and SEM are the same． In the case of uncalcined，the aver