城市污泥中总氮、总磷测定方法研究.docVIP

城市污泥中总氮、总磷消解方法研究 陈大勇 王里奥 马培东 欧阳鸥 陶玉 （重庆大学资源及环境科学学院，重庆 400044） 摘要：设计了正交实验并分析了H2O2与H2SO4消解污泥过程影响因素，在测定总氮时H2O2添加次数在α=0.1水平下具有显著性，而H2O2用量和H2SO4用量对总氮的测定影响较小，较优的消解方案为A3B1C1；在测定总磷时H2O2添加次数在α=0.01水平下具有显著性，H2O2单次用量在α=0.05水平下具有显著性，而H2SO4用量对总氮的测定影响较小，较优的消解方案为A3B1C3。综合考虑，总氮、总磷测定方法的最佳方案为为A3B1C3。按照该消解方案，测出总氮的回收率在98.53%-101.80% 关键词：城市污泥 总氮 总磷 消解 正交实验 中图分类号：X705 文献标识码 A 文章编号 The Digestion Method Research of Municipal Sewage Sludge’s TN and TP CHEN Da-yong, WANG Li-ao, (Chongqing University Institute of Resources Environment Science, Chongqing 400044 ) Abstract: Orthogonal experiment was designed and the impact factors were analyzed while municipal sewage sludge was digested by H2O2 and H2SO4. The adding times of H2O2 is significant at α = 0.1 level, but the dosage of H2O2 and H2SO4 has little impact to total nitrogen measurement, so the better digestion scheme is A3B1C1. The adding times of H2O2 is significant at α = 0.01 level, the dosage of H2O2 is significant at α = 0.05 level, but H2SO4 dosage has little impact to total phosphorus measurement, then the better digestion scheme is A3B1C3. General considerations, the best scheme of sludge digestion is A3B1C3 to measure TN and TP. According to the digestion program, the recovery rate of measuring TN is between 98.53% and 101.80%, while the recovery rate of TP is between 97.07% and 101.67%, so this method can accurately measure the sludge’s Key words: municipal sewage sludge TN TP digestion orthogonal experiment 随着社会的发展，城市人口的增加，工业废水与生活污水的排放量日益增多，污泥的产出量迅速增加 ADDIN EN.CITE EndNoteCiteAuthor李亚东/AuthorYear2005/YearRecNum347/RecNumrecordrec-number347/rec-numberref-type name=Journal Article17/ref-typecontributorsauthorsauthorstyle face=normal font=default charset=134 size=100%李亚东/style/authorauthorstyle face=normal font=default charset=134 size=100%李海波/style/authorauthorstyle face=normal font=default charset=134 size=100%梁浩/style/author/authors/contributorstitlestitlestyle face=normal font=default charset=134