高效液相色谱法测定地表水中4种紫外吸收剂的含量-食品安全质量.PDF

7 1 Vol. 7 No. 1 2016 1 Journal of Food Safety and Quality Jan. , 2016 - 4 朱绍华, 丁 利, 龚 强, 焦艳娜, 付善良, 成 婧, 王利兵* ( , , , 410004) 摘 要: 目的 - 4 。方法 , , 4 , , 结果 , (LOD)2.2~3.7 μg/L, 0.100~100 μg/mL, 72.6%~93.3%, (RSD)2.61%~4.37%结论 , , 关键词: ; ; ; Determination of 4 kinds of ultra-violet absorbents in surface water by solid phase extraction-high performance liquid chromatography * ZHU Shao-Hua, DING Li, GONG Qiang, JIAO Yan-Na, FU Shan-Liang, CHENG Jing, WANG Li-Bing (Technology Center of Hunan Entry-Exit Inspection and Quarantine Bureau, State Key Laboratory of Food Safety Testing, Hunan Key Laboratory of Food Safety Science Technology , Changsha 410004, China) ABSTRACT: Objective To establish a method for the determination of 4 kinds of ultra-violet (UV) absorbents in surface water by solid phase extraction-high performance liquid chromatography (SPE-HPLC). Methods The samples were purified and concentrated by solid phase extraction (SPE) after the optimization of solid phase extraction conditions. Four kinds of ultra-violet absorbents were detected by HPLC and the range of linearity, recovery, limits of detection and relativ