微波消解-ICP-MS测定酸角浸膏中的铅砷镉铬-食品安全质量检测.PDF

3 5 Vol. 3 No. 5 2012 10 Journal of Food Safety and Quality Oct. , 2012 -ICP-MS 1* 1 1 2 1 梁文君 , 梅春芬 , 陈 洁 , 谢爱群 , 张禹红 (1. , 650228; 2. , 650010) 摘 要: 目的 -(ICP-MS)方 法 , 结果 0~50.00 μg /L , 0.9995, : 2.0 μg /kg19.0 μg /kg 1.0 μg /kg9.0 μ g /kg, 81.5%~119.1%结论 , , , 关键词: ; ; ; ICP-MS Determination of lead, arsenic, cadmium and chromium in tamarindus concrete by microwave digestion system and inductively coupled plasma-mass spectrometry 1* 1 1 2 1 LIANG Wen-Jun , MEI Chun-Fen , CHEN Jie , XIE Ai-Qun , ZHANG Yu-Hong (1. Yunnan Entry-Exit Inspection and Quarantine Bureau Technology Center, Kunming 650228, China; 2. School of Chemical Science and Technology, Yunnan University, Kunming 650010, China) ABSTRACT: Objective To establish a method for the determination of lead, arsenic, cadmium and chro- mium by inductively coupled plasma-mass spectrometry. Methods The tamarindus concrete was digested in a microwave digestion system, and determined by external standard method. Results The method showed a good linearity over the range of 0~50.00 μg/L for Pb, As, Cd, and Cr with r 0.9995, and the detection limits were Pb 2.0 μg/kg, As 19.0 μg/kg, Cd 1.0 μg/kg and Cr 9.0 μg/kg, respectively. The mean recoveries ranged from 81.5%~119.1%. Conclusion This method is simple, rapid, and accurate, and it is suitable for the de