桂花精油缓释型香水及抗龋齿含片的研制-制药工程专业论文.docxVIP

华 华 中 科 技 大 学 硕 士 学 位 论 文 II II Abstract Essential oil is the main reason enduing fragrance to Osmanthus fragrans Lour., and it is also very valuable in medicinal use. At present, there are still some problems in the application of essential oil that the rate of the extraction is not satisfactory enough and high value-added products have been lacking, which extremely limit its application value in light industry and the field of health care oil. In this study, quality testing methods of essential oil of O. fragrans had been established, and its composition had been analized. Morever, conditions for extraction of essential oil had been optimized systematically. In addition, the products of the essential oil of O. fragrans were developed. The main results obtained in this study were listed as follows: Quality testing methods of the essential oil of O. fragrans had been established, and the physicochemical properties were analyzed. Meanwhile, GC-MS was used to identify its main components， including dihydro-β-Ionone, β- ionone, ethyl linolenate, palmitolei acid, etc. The optimal conditions of extracting essential oil from Osmanthus absolute were explored by uniform design for the first time. The optimal conditions obtained were: the ratio of O. absolute to 100% ethanol, 1:500 (m/v), the extraction temperature, 50 °C. With this method, the yield of essential oil of O. fragrans could reach 89.12 %. The key parameters of improving the yield of essential oil of O. fragrans were determined. A high quality recipe of Osmanthus- flavored perfume was gained, and high-quality use of essential oil of Osmanthus was developed. Weight loss and olfaction-based methods were combined to estimate the volatility time, and the function of vanillin in delaying volatile effect of O. fragrance was discovered. The results showed that when the concentration of the essential oil of O. fragrans was 3 - 4.5% (v/v), and the vanillin mass concentration reached to 0.15 g-0.23 g/100