立方相二氧化钕纳米棒的制备与表征.pdf

40 12 La O Al O 1713 2 3 2 3 40 12 Vol. 40 No. 12 2 0 1 2 1 2 JOURNAL OF THE CHINESE CERAMIC SOCIETY December 2012 ( 333001) Nd(Cit) X Nd(Cit)600 NdO2 NaCl 900 NdO2 NdO2 [220] O611.4 A 0454–5648(2012)12–1713–04 2012–11–29 10:09:55 /kcms/detail/11.2310.TQ1009.201212.1713_010.html Synthesis and Characterization of Cubic NdO Nanorods 2 ZHAO XueguoMIAO Lifeng (Jingdezhen Ceramic Institute, Jingdezhen 333001, Jiangxi, China) Abstract: NdO2 nanorods were obtained by calcinating Nd(Cit) complex, which was synthesized in citric acid solution via a ho- mogenous precipitation. The as-synthesized NdO2 nanorods were chararterized by X-ray diffraction and transmission electron mi- croscopy, respectively. The results show that the polycrystalline NdO2 nanorods can be obtained by calcinating Nd(Cit) complex in air at 600 , and the single crystalline NdO nanorods can be formed by calcinating the mixture of Nd(Cit) complex in molten NaCl at 2 900 . The results by high-resolution transmission electron microscopy indicated that the single crystalline NdO nanorods could 2 grow up along with the [220] direction. Key words: neodymium dioxide; nanorods; molten salt synthesis [11] [1–2] (AAO)