声发射法表征热障涂层的断裂韧性与损伤演化-材料科学与工程专业论文.docxVIP

II II Abstract Thermal barrier coatings (TBCs) have been the key thermal protection material of the engine due to their excellent thermal insulation, wear resistance, and corrosion resistance. However, due to the complex structure and the poor operation circumstance, the coating fracture and spalling often appears leading to coating failure and even catastrophic accidents. Therefore, the study of the TBC failure mode and critical mechanical parameters -surface fracture toughness and interface fracture toughness can provide the basis of the life prediction and reliability assessment, and it has become a concernful issue of research. In this paper, we use non-destructive testing methods (NDT) for monitoring the coating damage of TBC during three-point bend test and indentation test, to gain the critical mechanical parameter -fracture toughness. The main contents of this paper are as follows: Firstly, the expression of TBC’s surface fracture toughness under bending load was deduced. Then the TBCs’ injury process during bend test has been real-time monitored by acoustic emission technique (AE) and digital speckle correlation method (DSCM). The air plasma sprayed (APS) TBCs failure mode has been discussed under the bending load, and the critical thresholds were determined through the inflection points of the AE parameter and the strain. Inserting the critical thresholds into the theoretical model, the surface fracture toughness of as-received and oxidized TBCs were estimated as 1.005 MPa·m1/2 and 3.531 MPa·m1/2, respectively. The quantitative analysis of surface cracks was performed by acoustic emission parameter. The impact of oxidation on TBC surface failure was analyzed. Secondly, the theoretical models of indentation total cracks length method and acoustic emission parameter method to solve the surface fracture toughness of TBCs were introduced. The indentation tests of as-received and oxidized TBCs were monitored by AE technique to real-time. The differe