2-AZ31镁合金粉末氢气氛下机械球磨的组织演变.pdf

　A Z3 1 镁合金粉末氢气氛下机械球磨的组织演变 183 AZ31 镁合金粉末氢气氛下机械球磨的组织演变 Micro st r uct ure Evolutio n of A Z3 1 Magne siu m Alloy Pow der s Prep ared by Mechanical Milling in Hydro gen At mo sp here 王 　珩 ,胡连喜 ,陈先觉 ( 哈尔滨工业大学 材料科学与工程学院 ,哈尔滨 15000 1) WAN G Heng , HU Lianxi , C H EN Xianj ue ( School of Material s Science and Engineering , Harbin Institute of Technology , Harbin 150001 , China) 摘要 : 在氢气氛下机械球磨 A Z3 1 镁合金粉末 ,利用机械力作用使镁合金粉末与氢气发生反应生成纳米晶 Mg H2 ,用 X ( ) ( ) ( ) 射线衍射 XRD 、扫描电镜 SEM 和透射电镜 T EM 等方法观察和分析了镁合金粉末与氢气在球磨过程中的微观组织 演变 。结果表明:球磨初始阶段粉末颗粒被碾压成扁平状 ,随着球磨的进行粉末颗粒逐渐细化 ,球磨至 80h ,形成粒度 1 μ ～3 m 、晶粒尺寸 10nm 左右的纳米晶 Mg H2 粉末材料 。 关键词 : A Z3 1 镁合金粉末 ;机械球磨 ;纳米晶材料 ;Mg H2 ;微观组织 ( ) 中图分类号 : T G14622 　　文献标识码 : A 　　文章编号 : 100 14381 2008 100 18304 Abstract : A Z3 1 magne sium alloy pow der s were p rep ared by mechanical milling in a hydro gen at mo s p here . N anocry st alline M g H2 wa s creat ed by t he reaction of magne sium alloy pow der s and hydro gen at t ribut ed to t he mechanical force . The micro st r uct ure evolution of t he alloy durin g mechanical milling wa s charact erized by mean s of Xray diff ractio n ( XRD) , scanning elect ron micro scop y ( SEM ) and t ran smi ssion elect ron micro scop y ( T EM) , re sp ectively . The re sult s showed t hat ,during milling , t he pow der s were at fir st rolled into flake s , an d t hen , wit h t he f urt her increa sed of t he milling time ,t he