气相色谱-串联质谱法测定不同原产国抗草甘膦.PDF

7 9 Vol. 7 No. 9 2016 9 Journal of Food Safety and Quality Sep. , 2016 - * 何龙凉, 陈延伟, 陈智鹏 , 李小琴, 陈永欣, 杨怀军 (, 538001) 摘 要: 目的 -(gas chromatography- tandem mass spectrometry, GC-MS/MS) - , 方法 3 , , , , , (CAX ), , -, GC-MS/MS 结果 2.5~100 ng/mL (r0.999), 0.05 mg/kg 0.050.5 2.0 mg/kg 77.1%~96.5%, 8.8%(n=6)结论 , 关键词: ; ; ; - Determination of residues of glyphosate and its metabolite in roundup ready soybean imported from different original countries by gas chromatography-tandem mass spectrometry * HE Long-Liang, CHEN Yan-Wei, CHEN Zhi-Peng , LI Xiao-Qin, CHEN Yong-Xin, YANG Huai-Jun (Fangchenggang Entry-Exit Inspection and Quarantine Bureau, Fangchenggang 538001, China) ABSTRACT: Objective To detect the residues of glyphosate (PMG) and its metabolite-aminomethyl phosphonic acid (AMPA) in roundup ready soybean imported from different original countries in Fangchenggang port by gas chromatography-tandem mass spectrometry (GC-MS/MS), and analyze the differences. Methods Three batch samples of each country were collected from the roundup ready soybeans imported from the United States, Brazil, A