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19 1 No.1 Vol.19
2005 2 Journal of Chemical Engineering of Chinese Universities Feb. 2005
1003-9015(2005)01-0065-06
12, 2
(1. , 215011; 2. , 215006)
(A M)
(St-g-PVAm) 65 3hr (St-g-PAM) Hofmann
St-g-PVAm; PAM , 0 80
Hofmann St-g-PVAm
St-g-PVAm 65% St-g-PVAm 62% St-g-PVAm
Cu2+
(60~80 r⋅min− 1) 318 K St-g-PVAm 100~120 pH 6.0
Hofmann
TS236.9 O636.12 O633.21 A
Synthesis of Starch-g-Polyvinylamine and its Absorption Property
DONG Yan-mao1,2, LU Jian-mei2
(1.Department of Chemistry and Chemical Engineering, University of Science and Technology of Suzhou
Suzhou 215011, China;
2.Department of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006, China)
Abstract: Using cornstarch and acrylamide as crude materials and potassium persulfate as graft initiator
the starch-g-polyvinylamine(St-g-PVAm) was synthesized by two methods. In method one, St-g-PAM was
synthesized firstly under the condition of 65 and 3hr and then St-g-PVAm was synthesized with Hofmann
reaction. In method two, PAM was mixed with cornstarch which had been treated with NaOH, and then the
mixture was treated under the condition of 0 and 80 successively. During which the process of Hofmann
reaction and graft copolymerization was completed at the same time. Results show that St-g-PVAm can be
synthesized by these two metheds efficiently and the average grafting percentage of St-g-PVAm is 65% and
62% respectively. Meanwhile, the factors effecting on properties of absorption and flocculation of
St-g-PVAm were studied. Results show that St-g-PVAm absorbs metal-ion(Cu2+) efficien
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