6万吨乙丙橡胶生产工艺设计设计书.docxVIP

北京化工大学北方学院毕业设计 6 万吨/ 年乙丙橡胶生产工艺设计 高分子材料与工程专业 摘 要 乙丙橡胶， 统称乙丙弹性体， 是仅次于丁苯橡胶和顺丁橡胶的第三大合成橡 胶，是以乙烯、丙烯及乙叉降冰片烯 (ENB)为单体共聚而成。目前占世界合成橡 胶生产能力总量的 10%左右。乙丙橡胶以其优异的性能具有广阔的应用领域。除 了传统的汽车工业、防水建材、聚合物改性、油品添加剂、电线电缆、运动场地 及各类机械部件等应用领域外， 乙丙橡胶还可涉猎于食品包装、 抗微生物、 绝热 阻燃等弹性体制品领域。 本次设计年产 6 万吨乙丙橡胶装置聚合工段的工艺设计 , 乙丙橡胶聚合反应采用溶液聚合工艺， 使用的主催化剂为三氯氧钒， 辅助催化剂 为烷基铝， 溶剂为己烷。 在掌握生产原理、 聚合方法、 工艺流程等工作的基础上， 进行了物料衡算、热量衡算、 反应器等设备的相关计算；其中算得 E0203己烷 加热器的面积为 40.27 平方米 ，换热器管长为 6m，计算反应器 R0201的公称直 径为 5658mm高, 度为 9053mm，确定了聚合加料泵的扬程为 30.12m,以及 该泵的 轴功率 7.5kw,V0201 贮罐的总体积 37 立方米。并且绘制了反应器的管道布置图、 带控制点的流程图、编制了设计说明书等。 关键词：乙丙橡胶 溶液聚合 工艺设计 I 北京化工大学北方学院毕业设计 With an Annual Output of 60 Thousand Tons of Ethylene Propylene Rubber and Book Design. Abstract EPDM, generally called ethylene-propylene elastomer, and norbornene (ENB) as the monomer copolymerized with ethylene, propylene is the third major SR after SBR and BR. At present the production capacity of EPDM accounts for about 10% of the total production capacity of SR in the world. EPDM has wide range of application fields because of its excellent performance. Besides the traditional application fields such as auto industry, water-proof building materials, polymer modification, oil additives, electric wire and cable, athletic field and various mechanical parts, EPDM can also be used in food packaging, antimicrobial, heat insulation and inflaming retarding, and other elastomer products. It is annual output of 50,000tons of ethylene-propylene rubber device polymerization Section process design, the polymerization of ethylene-propylene rubber by solution polymerization process, the catalyst used for the vanadium oxytrichloride, vanadium, auxiliary catalyst is alkyl aluminum, solvent hexane. material balance, heat balance, reaction of a device such as the calculation finished based on the production principle of aggregation methods, process and other work ;including area of the hexane heaternamed E0203 is 40.27 square meters, length of heat exchangers tube is 6 meters, the diameter of the re