农业部783号公告-1-2006-水产品中硝基呋喃类代谢物残留量的测定液相色谱-串联质谱法.pdfVIP

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农业部783号公告-1-2006-水产品中硝基呋喃类代谢物残留量的测定液相色谱-串联质谱法.pdf

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ICS67.050 B 50 中华人民共和国国家标准农业部783号公告一1一2006 水产品中硝基峡喃类代谢物残留量的测定液相色谱一串联质谱法 Detemr inatino ofultroufranmeatbolicresiduesinaquaticProducts 勿 LC一MS/MSmehtod 0206一12一19发布 2006一12一19实施中华人民共和国农业部发布农业部873号公告一1一2006 目次前言 ················ ·······························································································…… 1 范围 ·································‘···· · · ········· ···················…·… 2 规范性引用文件 ····························································································一 3 原理 ······ ················································································‘‘·‘·· ··‘·‘二 4 试剂 ···‘ ·· ‘····· ·····················································································…… 5 仪器和设备 ·········‘·· ·················································································…… 6 测定步骤 6.1 样品处理 ·· ‘·············· · ·························································…… 6.2标准工作曲线制作 6.3 测定 6.4 空白试验 ··················· · ···············‘···· ················ 7 结果计算 8 方法灵敏度 ··········································································‘·············…… 9 方法回收率 ‘.·..··.······················································································…… 01 方法精密度 ····························· ············· ····‘··· ·····t·· ··· 附录A(资料性附录) 四种硝基吠喃代谢物中英文名称和缩写 ································…·… 附录B(资料性附录) 四种硝基吠喃代谢物混合标准(1.ong而止)特征离子质量色谱图 ·二附录C(资料性附录)空白鳗鱼样品特征离子质量色谱图·······························‘‘‘·一附录D(资料性附录) 鳗鱼添加样品特征离子质量色谱图农业部783号公告一1一0206 月U 舌本标准的附录A、附录B、附录C和附录D均为资料性附录。本标准由