碘量法测定气体放电后产生氧化剂的含量.docVIP

碘量法测定气体放电后产生氧化剂的含量 摘要 气体放电现象是一种常见的实验现象，本文是通过碘量法来测量其产生的氧化剂含量。碘量法是实验常见的氧化还原滴定法，他是利用碘单质的氧化性和碘离子的还原性来进行滴定的一种分析方法。实验中通过碘离子与氧化剂反应析出碘单质，然后用标定好已知浓度的硫代硫酸钠标准溶液对析出的碘单质进行滴定，计算出析出的碘单质的含量，最后利用析出的碘单质与氧化剂之间的定量关系，从而得到氧化剂的含量。标定硫代硫酸钠时，通过多次测量求其平均值的方法来减少实验误差，实验通过几组实验的对比，放气体放电后产生的氧化剂进行了测量，并对放电后的溶液利用紫外吸收光谱测量其吸光度，比较分析吸光度与氧化剂之间的关系 。论文从实验仪器的准备，碘量法的基本概念，实验原理，实验药品的配置，标准液的配置和标定，实验的方法步骤及，实验结果的计算分析及影响实验的因素全方位的对实验进行了阐述。 关键词：碘量法 含量 滴定 Abstract The gaseous discharge phenomenon is one kind of common experimental phenomenon, this article is the oxidant content which surveys it through the acidimetric to produce. The iodometric is the experimental common reduction method, he is carries on the titrate using the iodine simple substance oxide-ability and the iodine ion reducibility one analysis method. In the experiment through the iodine ion and the oxidant responded separates out the iodine simple substance, then with demarcates the good known density the sodium hyposulfite standard solution to the iodine simple substance which separates out to carry on the titrate, calculates iodine simple substance content which separates out, finally uses between the iodine simple substance and the oxidant quota relations which separates out, thus obtains the oxidant content. When demarcation sodium hyposulfite, asked its mean value through the multiple metering the method to reduce the experimental error, the experiment the oxidant which produced after the flourishing red Chinese pear-leaf crabapple solution and the neutral red solution electric discharge has separately carried on the survey, moreover had the oxidant content to the different discharge time to carry on the comparison. The paper from tests the instrument the preparation, the iodometric basic concept, the experimental principle, the experimental drugs disposition, the standard fluid disposition and the demarcation, the experimental method step and, the experimental result computation analyzed and affects experimental the factor unify-dir