《分析化学实验（下）》教学大纲.doc

课程编号： 课程名称：分析化学实验（下） 学分数：1.5 周学时数：3 课程内容：该实验课包括定量化学分析和仪器分析两部分实验内容基本操作，定量化学分析部分：首先进行基本操作训练，规范和熟练容量分析（酸碱滴定、配位滴定、氧化还原滴定及沉淀滴定法）、重量分析的基本操作，同时安排一定的实际样品分析，包括化肥、无机化工产品、水、矿石、金属等实际样品中主要成分的分析等，实验内容既有应用性又有综合性。仪器分析部分：主要安排原子光谱（吸收、发射）、分子光谱（红外、紫外、可见、荧光）、核磁共振谱、色谱（气相、液相）、电化学分析（电位、库仑、伏安）等实验内容，每个实验项目中主要包括分析方法原理、仪器结构、仪器操作方法、仪器输出信号的处理与分析及实际样品的分析应用等。 教材：(1) 武汉大学主编《分析化学实验》（第四版），高等教育出版社。 (2) 张剑荣等编，《仪器分析实验》，科学出版社。 Course code: Course name: Analytical chemistry experiments Credit: 1.5 Weekly class hour: 3 Introduction: The content of the experimental course includes the fundamental manipulation of the quantitative analysis and the instrumental analysis. The part of the quantitative analysis is to training students the basic manipulation of titrimetry (acid-base titrations, complexometric titrations, oxidation-reduction titrations and precipitation titrations) and gravimetry. At the same time, some practical samples such as fertilizer, inorganic chemical products, water, ore, metals etc are analyzed. In the part of instrumental analysis, the experiments of atomic spectrum (AAS, AES, AFS); molecular spectrum(IR, UV), NMR, chromatogram(GS, HPLC); electroanalytic methods (potentiometry, coulometry, voltammetry) are performed. The aim of the experiments is to make students understand the principles of analytic methods, the instrumental structures, the operations of the analytic instruments, the treatments and analysis of the instrumental output signal and the application for the real samples. Teaching material: （1）Analytical chemistry experiment (the 4th Edition), is edited by Wuhan University and published by Higher Education Press. （2）Instrumental analysis experiment, is edited by Zhang Jianrong et al., and published by Science Press.