电化学分析系统中pA~ μA 微电流测量.pdfVIP

1 第 25 卷 第 11 期 电子测量与仪器学报 Vol. 25 No. 11 · 972 · JOURNAL OF ELECTRONIC MEASUREMENT AND INSTRUMENT 2011 年 11 月 DOI: 10.3724/SP.J.1187.2011.00972 电化学分析系统中pA~μA 微电流测量 王 俊 (福州大学 至诚学院, 福州 350002) 摘 要: 为了提高电化学分析系统的分析速度和测量的准确度。探究如何对电化学分析系统中,既有慢变化又有快变化的 pA~μA 范围的微电流进行快速、准确的测量。基于定阻式 I/V 转换的方法,对 pA~μA 范围的微电流,设置了由微机控制的多个电 流量程及自动调零电路,以及从软､硬件上进行抗工频干扰的设计。实现对宽范围微电流测量的量程快速搜索､转换,提高了电化 学分析系统中 pA~μA 范围微电流测量的准确度｡ 关键词: 微电流; 测量; pA~μA; 电化学分析系统 中图分类号: TH399 文献标识码: A 国家标准学科分类代码: 460.40 pA~μA micro-current measurement in electrochemical analysis system Wang Jun (Zhicheng College, Fuzhou University, Fuzhou 350002, China) Abstract: In order to improve the speed of analysis and the accuracy of measurement in electrochemical analysis system, the fast-speed and accurate measurement of micro current of pA~μA range in both slow and fast change was researched. Based on the constant resistance I/V conversion method, for the pA~μA micro-current measurement range, a number of current computer control and automatic zero-adjusting circuit was set up, and anti-frequency interference design of software and hardware were carried out. The fast search and conversion in wide micro current measurement range were realized. Thereby the scope of pA~μA micro-current measurement accuracy is enhanced. Keywords: micro-currents; measurements; pA~µA; Electrochemical analysis system 度之关键在于对微电流的测量。 1 引 言 鉴于微电极、超微电极其尺寸及表面形状、测 应用在电化学、生物电化学和生命科学等作为