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中国科技论文在线
Synthesis of CdS-PAEK nanocomposite#
**
Zhang Yinan, Jiang Dong, Qin Hongyi, Zhang Haibo, Jiang Zhenhua
(College of Chemistry, Jilin University, ChangChun 130012)
5 Abstract: In the present research it is reported the synthesis and characterization of Poly (arylene ether
ketone) (PAEK)-cadmium sulfide nanocomposites prepared using carboxylic-functionalized poly
(arylene ether ketone) (PCA-PAEK) as the ligand in DMF solutions from Cd(Ac)2 and thiourea. The
resulting CdS/PCA-PAEK nanocomposites were characterized by fourier transform infrared
spectroscopy, X-ray diffraction, transmission electron microscopy, UV-visible spectroscopy,
10 photoluminescence spectroscopy, confirming the formation of CdS QDs with small particle size with
structure. The results of photoluminescence measurement showed that the nanocomposite exhibited
distinct luminescence properties. Furthermore, the effects of reaction time, CdS/PCA-PAEK ratio and
Cd2+/thiourea ratio on the photoluminescence of CdS QDs were also investigated. Thus, a novel simple
route was successfully developed for synthesizing nanohybrids based on quantum dots and high
15 performance polymers with incorporated carboxylic moiety.
Keywords: nanocomposites; CdS; PAEK
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