水产品中多聚磷酸盐含量的离子色谱测定方法 英文意见稿.docVIP

 Foreword Annex A of this standard is an informative annex.。 This standard was proposed by and is under the charge of the Certification and Accreditation Adminstration of the Peoples Republic of China. This standard was drafted by the Shandong Entry-Exit Inspection and Quarantine Bureau 、 Entry-Exit Inspection and Quarantine Bureau and Jiangsu of the Peoples Republic of China. This main drafters of this standard are: Cuihe, Chen xiaomei, Liu jingjing, ,Wang jun, Jiao hongqiang, Lv peng, Mao xubin, Zhang xiaowen. This standard is a professional one which is promulgated for the first time.  Method for the determination of polyphosphates in aquatic products by ion Chromatography 1 Scope This standard specifies the method of sample preparation and determination of polyphosphates in aquatic products, such as Cod-fishing, scallop, shrimp, fish rotten produce. This standard is applicable to the determination and confirmation of polyphosphates in aquatic products, such as Cod-fishing, scallop, shrimp, fish rotten produce. Reference Items in following text would become items belong to this text via reference in the relative part. For files without an indication of date, the last version would be applicable in the text. GB/T 6682 Specification and test method for water used in analytical lab (neq ISO 3696:1987) GB/T 603 Chemical reagent Preparations of reagent solutions for use in test methods (GB/T 603-2002,ISO6353-1；1982,NEQ) 2 Principle The test sample is extracted with water, after destroied enzyme active in sample with boiled water, then the extract is detected by ion Chromatography. 3 Reagent and material Unless specifically noted, all reagents used should be A.R.and “water” is deionized water correspinding to GB/T 6682. 3.1 Pure water (resistance ratio ≥ 18.2MΩ/cm ) 3.2 Sodium hydrxide: G.R. 3.3 Polyphosphates: Natrium phosphate, Natrium pyrophosphate, Natrium tripolyphosphate, Natrium trimetaphosphate are A.R. 3.4 Standard stock solution 3.4.1 Standard sto