微波辅助-旋转回流提取叶下珠中的没食子酸.pdfVIP

第22卷第 1期 化 学 研 究 与 应 用 V01．22．No．1 2010年 1月 ChemicalResearchandApplication Jan．，2010 文章编号：1004—1656(2010)O14)1244)5 微波辅助一旋转回流提取叶下珠 中的没食子酸 韦寿莲H，严子军 ，刘 玲 ，邓光辉 (1．肇庆学院化学化工学院，广东 肇庆 526061； 2．广西民族大学化学与生态工程学院，广西 南宁 530006) 关键词：微波辅助旋转回流提取；叶下珠 ；没食子酸 ；毛细管电泳 中图分类号：0657．8 文献标识码：A M icrowave-assistedcircumrotationrefluxextraction ofgallic acidfrom PhyllanthusUrmariaL WEIShou—limah YANZi-jun，LIULing，DENGGuang—hut ， (1．FacutyofChemistryandChemicalEngineering，ZhaoqingUniversity，Zhaoqing526061； 2．CollegeofChemistry＆EcologicalEngineering，GuangxiUniversityforNationalities，Nanning530006) Abstract：A newkindofmi crowave。assistedcireumrotationrefluxextractiondeviceWas constructedandusedtostudytheextraction technologyofgallicacidfrom phyllanthusurmad~L．Theextractionprincipleofthedevicewassameasthatofmicrowave-assisted solventextractionbutusingcircumrotationtechniquesasauxiliarystirrertoaccelerate theprocess．CapillaryelectrophoresisWas usedtodeterminategallicacidinphyllanthusurmariaLextractsinordertoevaluatetheextractionefficiencyofthemethod．Itwas foundthatthe mostimportantfactors influencing extraction gallicacid were solventkind and microwavepower．The optimum extractionconditioriswereasfollows：waterusingas solvent，solid—liquidratio1：30(g：mL)，microwavepowerlowrailandirradiate time4minute．Undertheoptimum extractionconditions，fiveexperimentswerecarriedoutandtheaverageextractionrateofgallic acidinph)llanthusurmariaLwas4．32mg／g，relativestandarddeviations(R．S．D．)was2．2％．Comp~edwithotherextraction methodse．g．refluxextractionandmicrowave-assistedextraction，betterextractionefficiencywasobservedofrhtemicrowave-assisted circumrotationrefluxexrtaction． Keywo