山芝麻化学成分和两面针新棒状花椒酰胺分离研究.pdf

目 录 中文摘要······················································1 英文摘要···························································3 引 言····························································5 正 文····························································7 第一部分 山芝麻的化学成分研究···························7 1 药材、仪器和试剂·····························································7 1.1 原料药材浸膏·······················································7 1.2 实验仪器·······················································7 1 . 3 试剂··················································7 2 化学成分预试验····················································8 2.1 药材浸膏预实验结果················································8 2.2 化学成分预试小结·············································10 3 山芝麻的分离及其流程图········································10 3. 1 山芝麻正丁醇水不溶部位的分离··························1 0 3.2 山芝麻乙酸乙酯部位的分离········································10 3.3 山芝麻化学成分提取与分离流程图································11 4 单体化合物的结构鉴定·············································12 4.1 化合物Ⅱ的结构鉴定··············································12 4.2 化合物 III 的结构鉴定·············································17 4.3 化合物Ⅳ的结构鉴定··············································17 4.4 化合物 V 的结构鉴定··············································25 4.5 化合物 VI 的结构鉴定·············································32 5 小结············································································37 第二部分 两面针新棒状花椒酰胺的分离研究······························38 1 药材、仪器和试剂·······················································38 1.1 两面针药材的鉴定··················································38 1.2 仪 器 、 试 剂························································································ ··38 2 三种试剂提取实验方法和步骤············································39 2.1 甲醇提取实验····················