无糖型复方扶芳藤合剂研制及质量控制方法研究.pdf

目 录 中文摘要··················································1 英文摘要 ··················································4 引言 ·····················································8 正文 ····················································10 第一部分 无糖型复方扶芳藤合剂的提取工艺研究 ············10 第一节 无糖型复方扶芳藤合剂水提工艺参数的优化研究 ········10 1 实验材料···············································10 1.1 实验药材 ·············································10 1.2 实验试药··············································11 1.3 主要仪器 ··············································11 1.4 分析软件 ··············································11 2 实验方法 ···············································11 2.1 正交实验设计 ··········································11 2.2 药材提取方法 ··········································11 2.3 含量测定方法 ··········································12 2.3.1 色谱条件 ············································12 2.3.2 对照品溶液的制备 ····································12 2.3.3 供试品溶液的制备 ····································12 2.3.4 样品测定 ············································12 2.4 得膏率的测定 ··········································13 3 实验结果 ···············································14 3.1 正交实验结果 ··········································14 3.2 正交实验结果方差分析 ··································14 4 正交实验结果验证性实验 ································15 5 结论 ··················································15 1 第二节 无糖型复方扶芳藤合剂醇提工艺参数的优化研究 ·······16 1 实验材料 ··············································16 1.1 实验药材··············································16 1.2 实验试药··············································16 1.3 主要仪器 ··············································17 1.4 分析软件 ··············································17 2 实验方法 ···············································17 2.1 正交实验 ··············································17 2.1.1 正交实验设计 ········································17 2.1.2 正交实验结果 ·······