羽裂华蟹甲草根化学成分研究.pdfVIP

′06 陕西药物分析学术研讨会 羽裂华蟹甲草根化学成分的研究 1 2 1 3 2 何仰清 魏小梅 姚秉华 马占营 高黎明 ( 1. 西安理工大学应用化学系 西安 710054 ；2.西北师范大学化学化工学院，兰州 730070 ；3. 咸阳师范学 院化学系，咸阳 712000) 摘要 目的：对羽裂华蟹甲草的根进行化学成分的研究。方法：溶剂萃取、色谱法分离化学 成分，波谱法鉴定其结构。结果：从根中分离得到 6 个化合物，硬酯酸（1），正十六酸（2 ）， 常春皂甙元-3-O-α-L-吡喃鼠李糖基（1→2 ）-α-L-吡喃阿拉伯糖甙（3 ），Acteoside(4) ，β-谷 甾醇（5 ），β-谷甾醇甙（6 ）。结论：化合物 3，4 首次从羽裂华蟹甲草中得到，并且为首次 报道该植物的化学成份。 关键词：羽裂华蟹甲草 化学成分 甾醇化合物 Study on the chemical constituents of the roots of the Sinacalia tanutica maxin 1 2 1 3 2 HE Yang -qing , WEI Xiao -mei , YAO Bing-hua , MA Zhan-ying , GAO Li -ming 1 2 ( Department of Applied Chemistry, Xi’an University of Technology, Xi’an 710054; Department of Chemistry, Key Laboratory of Polymer Materials of Gansu Province, Northwest Normal University, Lanzhou 730000; 3Department of Chemistry, Xianyang Normal University, Xianyang 712000) Abstract Objective ：To study the constituents from the roots of Sinacalia tanutica (maxin). Methods: The constituents were isolated and purified with Chromatographic methods, identified by NMR, MS and IR. Result: six compounds were isolated, stearic acid(1), hexadecanoic acid(2), hederagenin-3-O-α-L-rhamnopyanosyl(1→2)-α-L-ar-abinopranoside(3),Acteo-side(4),β-sitosterol (5), daucosterol(6). Conclusion: Compounds(3) and (4) were isolated for the first time from S. tanutica (maxin ) and this is first time reported on the constiutents of this plant. Key words: sinacalia tanutica maxin, chemical composition, sterol compounds 羽裂华蟹甲草（Sinacalia tangutica maxim ）为菊科（compositale ）华蟹甲草属（Sin