硅藻土的分离和其负载氧化铁后可见光光催化抗菌性能研究.pdfVIP

（4）特种功能材料 硅藻土的分离及其负载氧化铁后 可见光光催化抗菌性能研究 1 2 1 1 2 1， 陈晶 ，杨婷 ，李松 ，任玉平 ，王建华 ，秦高梧 * 1 东北大学材料各向异性与织构教育部重点实验室，沈阳，110819 2 东北大学理学院，沈阳，110819 摘 要：采用饱和蔗糖溶液为溶剂，通过低速离心，可去除硅藻土中的杂质和破碎小颗粒，对其进行分离。 同时研究了不同煅烧温度对硅藻土比表面积和表面化学性质的影响。结果表明，600℃以下煅烧对硅藻土的 比表面积影响甚小，800℃以上温度煅烧不仅明显降低其比表面积，而且硅藻土表面出现去羟基化。当硅藻 土表面负载上一定浓度的Fe O 纳米颗粒后，其在可见光下的光催化杀菌率可达到96.2% 。 2 3 关键词：硅藻土；分离；光催化；氧化铁；杀菌率 Separation of diatomite and visible light responsed photocatalytic bactericidal performance of diatomite loaded with Fe O nanoparticles 2 3 CHEN Jing 1, YANG Ting 2, LI Song 1, REN Yuping 1, WANG Jianhua 2 , QIN Gaowu1,* 1 Key Laboratory for Anisotropy and Texture of Materials (MOE), Northeastern University, Shenyang 110819 2 College of Sciences, Northeastern University, Shenyang 110819 *Corresponding author, E-mail: qingw@ Abstract：Diatomite was separated by wiping off impurities and fragments by means of selecting sat urated sucrose solution as solvent and centrifuging at low speed. The effect of calcination temperature on specific surface area and surface chemistry of diatomite was also investigated. The results show that the specific surface area is little affected when the calcination temperature is lower than 600 ℃, and it decreases rapidly when the calcination temperature is higher than 800 ℃, together with de-hydroxylation of diatomite surface. When diatomite is loaded with certain concentration of Fe O nanoparticles, its photocatalytic bactericidal rate can be up to 96.2% by visible 2 3 light irr