湿磨工艺对锶铁氧体预烧料性能的影响.pdfVIP

工艺·技术·应用 湿磨工艺对锶铁氧体预烧料性能的影响 1 1 2 2 2 林海恋 ，王 忆 ，温东强 ，李金道 ，吕兆民 （1. 五邑大学 应用物理与材料学院，广东江门 529020 ； 2. 广东江粉磁材股份有限公司，广东江门 529020 ） 摘 要：通过传统的陶瓷工艺制备锶铁氧体预烧料，研究了湿磨工艺对锶铁氧体预烧料性能的影响。结果 表明，碳酸锶一次湿磨时间对碳酸锶和预烧料粒度影响较大，不同湿磨工艺下预烧料微观结构差异较大，饱和 磁化强度随碳酸锶一次湿磨时间的延长先增大后减小。当碳酸锶一次湿磨时间为 2.5h 时，样品形貌呈六角片状， 致密性较好，并且 M 2 s 较优，为 72.09 A·m /kg 。 关键词：锶铁氧体；预烧料；湿磨工艺；微观结构；饱和磁化强度 中图分类号： TM277+ .5 文献标识码： A 文章编号：1001-3830(2015)01-0069-03 Effects of wet milling process on the performance of pre-sintered strontium ferrite 1 1 2 2 2 LIN Hai-lian , WANG Yi , WEN Dong-qiang , LI Jin-dao ，LV Zhao-min 1. School of Applied Physics and Material , Wuyi University, Jiangmen 529020, China; 2. Jiangmen City Powder Metallurgy Factory, Ltd, Jiangmen 529020, China Abstract ：Pre-sintered strontium ferrite was prepared by traditional ceramic process. The effect of wet milling process on the properties of pre-sintered strontium ferrite was studied. The results show that wet milling time has a great influence on particle size of strontium carbonate and pre-sintered powder, pre-sintered power has different microstructure for different wet-milling process conditions, and Ms increase firstly and then descrease with milling time. When milling strontium carbonate for 2.5 h, sample is obtained with hexagonal sheet structure, higher density and Ms of 2 up to 72.09 A·m /kg. Key words ：strontium ferrite; pre-sintered powder; wet milling process; microstructure; saturation magnetization 个很重要的原因是主要原料粒度的不均匀性。这是 1 引言