Potentiostatic deposition process of fluoride conversion film on AZ31 magnesium alloy in 0.1 M KF solution.pdf
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Potentiostatic deposition process of fluoride conversion film on AZ31 magnesium alloy in 0.1 M KF solution.pdf
Electrochimica Acta 105 (2013) 554–559
Contents lists available at SciVerse ScienceDirect
Electrochimica Acta
j o u r n a l h o m e p a g e: w w w. elsev /locate/elec t a c ta
Potentiostatic deposition process of fluoride conversion film on AZ31
magnesium alloy in 0.1 M KF solution
Liping Wu, Junhua Dong ∗ , Wei Ke
State Key Laboratory for Corrosion and Protection, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
a r t i c l e i n f o a b s t r a c t
Article history: The coating process of fluoride conversion film deposited at −1.4V on AZ31 Mg alloy in 0.1 M KF solution
Received 8 March 2013 of pH 7.5 at room temperature was studied by in situ potentiostatic polarization, together with scanning
Received in revised form 29 April 2013 electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), X-ray diffraction (XRD) and X-
Accepted 30 April 2013
ray photoelectron spectroscopy (XPS). Our results show that the coating process can be distinguished
Available online 21 May 2013
into five stages. The initial two stages are caused by the rapid discharge of the electrical double layer
capacitance and the slow increase of the faradaic current density on AZ31 Mg alloy and Mg(OH)2 was
Keywords:
detected in the corrosion product at these stages. The third process corresponds to the deposition of
AZ31 magnesium alloy
Fluoride conversion film
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