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Novel synthesis of nickel oxide microsphere with high surface area and its catalytic application for carbon dioxide reforming of methane.pdf

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Novel synthesis of nickel oxide microsphere with high surface area and its catalytic application for carbon dioxide reforming of methane.pdf

J．Cent．SouthUniv．(2014)21：1747—1751 DoI：l0．1007／s1l771—014．2】19—9 鱼Springer Novelsynthesisofnickeloxidemicrospherewithhighsurfaceareaandits catalyticapplicationforcarbondioxidereformingofmethane wuxu(吴旭)，WUZheng—huang(武正簧)，ANXia(安霞)，XIEXian—mei(谢鲜梅) CollegeofChemistryandChemicalEngineering，TaiyuanUniversityofTechnology,Taiyuan030024，China ◎CentralSouthUniversityPressandSpringer-VerlagBerlinHeidelberg2014 Abstract：Nickeloxide(NiO)microspherewithalargesurfaceareawasnovellysynthesizedthroughnickelbicarbonateN(i(HCO 1 precursor．Theobtainednickeloxide(NiO)microspherewascharacterizedbyX—raypaRemdiffraction．scanningelectronmicroscopy, CO2temperature—programmed desorption，H2temperature-programmedreduction，N2adsorption／desorption and laserscattering particlesizedistributionanalyzer．Itwasfoundthatnieke1oxide(NiO)synthesizedbythetherlTlaldecompositionofNi(HCO1 throughareahydrolysis，presentedverynicemicrospherewithhighsurfacearea．Thecatalyticpropertiesofobtainednicke1oxide fNiO)microsphereweresutdiedinthereactionofcarbondioxidereformingofmethanewhere91．3％conversionofCHdwith93％ conversionofCO，wasobserved．Besides，thecatalystmaintainedhighstabilityover200honthestream． Keywords：synthesis；NiOmicrosphere；largesurfacearea；catalysis spaceofrthereactantsandproducts．YANG 8『1eta1 1IntrOductiOn reported nano—nicke1 oxide particles through the hydrolysisofnickelacetateprecursorinamixedsolvent 0fparticularjnteresttomaterialsresearchersisthe ofwaterand glycero1．Meantime，KUANG 9『1etal factmatmicrospherestructureshavehighersurfaceareas prepared layered．sturcture nickeloxide microspheres thanconventionalmaterials．Theimpactofmicro