萘系高效减水剂的合成研究与生产设计论文.docx

摘要混凝土是当今世界用量最大、用途最广的工程材料之一。随着 21 世纪混凝土工程的大型化、多功能化、施工与应用环境的复杂化、应用领域的扩大化以及资源与环境的优化，人们对传统的混凝土材料提出了更高的要求，混凝土材料的高性能化和高功能化已成为 21 世纪混凝土材料科学与工程技术研究的重点和方向。本文详细介绍了常用高效减水剂的结构类型、性能特点及国内外的研究应用现状，分析了萘系高效减水剂发展状况及存在的问题。利用单因素法系统地研究了萘原料的含量、硫酸品种、各个步骤中的反应物配比、反应时间、反应温度、酸度、加料方式等工艺参数及降低产品中硫酸钠含量对萘系高效减水剂性能的影响，确定了合成萘系高效减水剂最佳工艺条件。以最优的合成工艺条件用于工业生产，提高了生产效率、提高了产品的性能及适应性、降低了产品的成本。作者还对萘系高效减水剂进行产品的性能研究，并在应用方面与其他产品进行了净浆流动度、抗压强度比较，同时还对产品在减水率、泌水率、坍落度经时损失等方面进行研究。根据相应的国家标准和行业标准，作者对采用最佳工艺条件合成的萘系高效减水剂产品进行了系统的性能测试，结果表明，采用此工艺条件生产的产品能达到或超过国家一等品的标准。本课题就年产 1000 吨萘系高效减水剂生产作了工艺流程的设计、工艺计算及设备的计算与选型等工作，以及萘系高效减水剂生产过程中的环境保护、技术经济分析，对萘系高效减水剂的工业生产具有一定的指导意义。关键词：萘系高效减水剂；合成研究；产品性能；应用研究；设计IAbstractConcrete is one of the most employed engineering materials all over the world withits quantity and its abroaden application. Traditional concrete was put forward moreand more requires along with large scale, multi-function, construct complication,widen application, resource and environment optimization of concrete project. Highperformance and high function is the research emphasize and direction of concretematerial and its engineering technology in 21 century.In this paper, the structure types, performance characteristics and the situationsof resarch and application of commonly used superplastieizers at home and abroadwere introduced in detail. The development condition and the problems in practice ofNaphthalene series supeiplasticizer were also analysed.By using the mono-factor method, the influences of the process parameters,such as material purity, material ratio, the decreasing content of the sodiumsulfate ,the reaction time and temperature every stage and the reaction acidity etc.on the performance of Naphthalene series superplasticizer were studiedsystematically.the optimal synthesizing process condition were obtained. Using theoptimal synthesizing process condition in production, the production efficiency, theproduct performance and the product adaptability were improved, the product costware debased also.The performance of