QTools Data Analysis Training培训教程文件.pptVIP

* * * * * * * * * * * * * * * * * * * Viscoelastic model - References Domack et al., Physical Review E, 56 (1997) p680 Discusses viscoelastic profiling of polymer films on quartz resonators. Mathematic relations are described. Voinova et al., Physica Scripta, 59 (1999) p391 Same mathematic relations, including D-factor discussion. Irwin et al., Langmuir, 21(12) (2005) p5529 Good example of Q-Tools modeling, applied on polymer films Vogt et al., J. Phys. Chem. B 108 (2004) p12685 Discussion on validity of Sauerbrey, comparison with model Snabe et al., Chem. and Phys. of lipids 133 (2005) p37 Example of modeling: lipid film degradation Ex situ coating Acquire baseline in air Acquire baseline in liquid in seperate file Take the sensor out and coat it Acquire new baseline in air Acquire new baseline in liquid and perform measurement Use stitch function in QSoft. Operating range 100 101 102 103 104 105 106 107 108 Lab viscometers QCM-D Modeled output based on a narrow frequency window Data from lower frequency range cannot necessarily be compared with QCM-D modeled data. Hz Open QSoft file in QTools Go to Modeling/New Model/Viscoel.... Include layers, include f and D values Go to ”parameters” Set parameters Go to ”measured data” Click ”estimate all” Go to ”fit settings” Click ”limit x-values” if wanted Pull curtain to limit x-values Click ”Fit all” The tab ”Fit analysis” appears The tab ”Vector parameter plot” appears * Hello everyone, you will be able to read clarifying text in this space for each slide in this presentatation! * * * * Within biomaterials research and development, hydroxyapatite (HA) is well known for its biocompatible properties, particularly in bone bonding, and for its potency of rapid integration into the human body. Orthopaedic and dental devices are often coated with HA to facilitate integration and acceptance by human tissue. An interesting example of studies on protein behavior onto HA using QCM-D, is the work carried out by a group of