原创力文档freeze-thawing treatment on the microstructure and thermal properties of corn starch granule.pdf
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freeze-thawing treatment on the microstructure and thermal properties of corn starch granule
RESEARCH ARTICLE
Effect of freeze-thawing treatment on the microstructure and
thermal properties of non-waxy corn starch granule
Shifeng Yu1,2, Yongchun Zhang1, Hongyan Li 2, Yan Wang1, Chunyu Gong1, Xiaolan Liu1, Xiqun Zheng1
and Narasimha Kumar Kopparapu1
1College of Food and Bioengineering, Qiqihar University, Qiqihar, P.R. China
2Centre for Nutrition and Food Sciences, Queensland Alliance for Agriculture and Food Innovation, The University of
Queensland, Brisbane, Queensland, Australia
In the present study, non-waxy corn starch was processed by different freeze-thawing
temperatures and cycles. The effects of freeze-thawing treatment on the surface structure,
granules particle size, Maltese crosses, crystalline, and thermal properties of non-waxy corn
starch were investigated. The number of pores on the surface of starch granules increased with
freeze-thawing cycles. The granule size, crystalline intensity and degree, gelatinization
temperatures, and enthalpy values of corn starch decreased with freeze-thawing cycles
increased. The Maltese crosses indicated that loss of Maltese cross increased when freeze-
thawing cycles increased, but decreased with increase in temperature. Moreover, clear cracks and
big pores were observed on the surface of starch granules, and smaller granule size and lower
thermal parameters were obtained in the distorted corn granules caused by the changes in
crystalline structure under appropriate treatment (20°C freezing and 25°C thawing, 20 cycles).
Freeze-thawing treatment significantly increased the porosity of corn starch, which indicated that
it can improve adsorptive capacity of starches. Therefore, freeze-thawing method is potentially
very useful to produce porous starch as carrier or absorbent for food and medicine. These
findings could have important applications in starch modification industry.
Received: May 3, 2015
Revised: June 21, 2015
Accepted: June 24, 2015
Keywords:
Corn starch / Freeze / Granule / Thawing / Thermal proper
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