Evodia#39;s 1H NMR fingerprint analysis.docVIP

 PAGE \* MERGEFORMAT 15 Evodia#39;s 1H NMR fingerprint analysis 【Abstract】 Objective To Evodia Evodia rutaecarpa (Juss.) Benth.’s 1H  NMR fingerprints for resolution. Methods silica gel column chromatography of SCEA and SCEB Evodia chemical composition, identification of its structure, and SCEA and SCEB for 1H-NMR studies, in order to achieve Evodia the 1H  NMR fingerprint analysis. Results Evodia SCEA, 1H  NMR fingerprints of the main display evodiamine, rutaecarpine, dehydroevodiamine 3 compounds characteristic resonance signals, Evodia SCEB of 1H  NMR fingerprints of the main features of resonance signals show dehydroevodiamine. Samples from different sources of its 1H-NMR fingerprinting has good reproducibility and characteristic. Conclusion Evodia the 1H  NMR fingerprint identification can be the source of its base. Keywords: Wuzhuyu 1H  NMR fingerprint Studies on 1H  NMR Fingerprints of Evodia rutaecarpa (Juss.) Benth. Abstract: ObjectiveTo analyse the 1H  NMR fingerprints of Evodia rutaecarpa (Juss.) Benth. MethodsThe chemical constituents were obtained from SCEA and SCEB of Evodia rutaecarpa (Juss.) Benth. By chromatography on Silica gel column. The characteristic signals of the 1H  NMR fingerprints were analysed after determining the structures of the compounds isolated from SCEA and SCEB. Results1H  NMR fingerprints of the samples of Evodia rutaecarpa (Juss.) Benth. which were collected from different regions showed high characteristic features and reproducibility. Three main compounds from SCEA were elucidated by spectral analysis as evodiamine, rutaecarpine and dehydroevodiamine respectively and the main compounds from SCEB were elucidated by spectral analysis as dehydroevodiamine. ConclusionThe 1H  NMR fingerprints of Evodia rutaecarpa (Juss.) Benth. might be utilized for the original authentication of the plant. Keywords:: Evodia rutaecarpa (Juss.) Benth.; 1H  NMR fingerprint Rutace