High-performance liquid chromatography compound Gastrointestinal good Capsule paeonol.docVIP

 PAGE \* MERGEFORMAT 7 High-performance liquid chromatography compound Gastrointestinal good Capsule paeonol Author: Zheng Ya-yu, Jin Fengyun, Yichun Sun, Jie Huang, Mark Qin [Abstract] Objective To establish a good capsule gastrointestinal compound method for the determination of paeonol. Method using ultrasonic extraction method to extract the compound Gastrointestinal good capsules, and use high-performance liquid chromatography assay of paeonol. Results Paeonol in between 0.1 ~ 0.5 μ g and the peak area showed good linear relationship, r = 0.999 9, average recovery was 100.14%, RSD of 0.95% (n = 5). Conclusion High Performance Liquid Chromatography paeonol method is sensitive and reproducible. [Keywords:] compound Gastrointestinal Capsule Paeonol good ultrasonic extraction high-performance liquid chromatography Gastrointestinal capsule from the compound Jia Xu Changqing, spiced blood rattan, Evodia, in September of Health and other medicinal composition, the region in Guizhou Southeast Guizhou Miao people used to treat stomach, and the application of more extensive, with Qufeng blood circulation, qi analgesic efficacy in clinical practice for the treatment of superficial gastritis, atrophic gastritis, stomach pain, gastric ulcer, duodenal ulcer and so on. Modern research table Mingdan Pi phenol with anti-bacterial and anti-inflammatory effect, for good gastrointestinal capsule compound, one of the active ingredients. In this experiment, high-performance liquid chromatography Gastrointestinal good capsule of compound contained in the determination of paeonol conduct research. An instrument and reagent Instrument: Agilent-1100 high-performance liquid chromatography Yee (binary pump, DAD detector). HPLC pure methanol, water re-distilled water, other reagents were of analytical grade. Paeonol reference substance (Lot No. :0708-9704) from China provided medicines and biological products. 2 Methods and Results 2.1 Chromatographic conditions With 18 alkyl