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HPLC Determination of ginsenoside capsules heart Shukang Rg1 Re content of
PAGE \* MERGEFORMAT 7
HPLC Determination of ginsenoside capsules heart Shukang Rg1 Re content of
[Abstract] Objective: To establish cardiac Shukang capsule ginsenoside Rg1 and Re contents determination. Methods: The high-performance liquid chromatography (HPLC), stationary phase: C18 column, mobile phase: acetonitrile -0.05% phosphoric acid (1:4); detection wavelength of 203nm, measured heart Shukang Capsule Ginsenoside Rg1, Re, of the content. Results: The method determination of ginsenoside Rg1, Re the linear range of 1.0-10.0μ g, its recovery was 95.3-100.4%, precision of ≤ 2%. Conclusion: The method is simple and accurate for heart Shukang capsules provide a reference method for the determination.
[Keywords:] Heart Shukang capsules; ginsenoside Rg1, Re; high-performance liquid chromatography
Heart Shukang capsules from 37, red sage root, astragalus and other traditional Chinese medicine composition, method of extracting active ingredients scientifically crafted for Yiqihuoxue complement the heart and brain, for me, the experience of hospital treatment of cardiovascular diseases side. Of which 37 (Radix et rhizoma notoginseng) is a rare traditional Chinese medicine in China, the main active ingredient for a variety of saponin, and has a variety of significant pharmacological effects, including 37 of the compound preparation of regular composition of its assay as an indicator.
Using high performance liquid chromatography method on cardiac Shukang capsule ginsenoside Rg1, Re had determination. In the sample pretreatment, the use of macroporous resin adsorption separation directly on the sample extract for purification, using C18 column and acetonitrile -0.05% phosphoric acid (1:4) as mobile phase, detection wavelength of 203nm, can obtain satisfactory results.
1 Materials
1.1 Instrument Waters 515 high-performance liquid chromatography, Waters Millennium32 chromatography workstation. Turn evaporator (Shanghai Qingpu Huxi Instrument Factory), FQC 1
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